7-Octen-3-one, 6-(dimethylphenylsilyl)-, O-methyloxime

Base Information

Chemical Name:7-Octen-3-one, 6-(dimethylphenylsilyl)-, O-methyloxime
CAS No.:914928-09-9
Molecular Formula:C17H27NOSi
Molecular Weight:289.493
Hs Code.:

Synonyms:

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Chemical Property of 7-Octen-3-one, 6-(dimethylphenylsilyl)-, O-methyloxime

Chemical Property:

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Technology Process of 7-Octen-3-one, 6-(dimethylphenylsilyl)-, O-methyloxime

There total 6 articles about 7-Octen-3-one, 6-(dimethylphenylsilyl)-, O-methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-(dimethyl-phenyl-silanyl)-oct-7-en-3-one

: 593-56-6
N-methoxylamine hydrochloride

: 914928-09-9
6-(dimethyl-phenyl-silanyl)-oct-7-en-3-one O-methyl-oxime

Guidance literature:: With sodium acetate; In ethanol; water; at 60 ℃; for 2h;
DOI:10.1021/ol061914e

Reference yield:

: 768-33-2
phenyldimethylsilyl chloride

: 914928-09-9
6-(dimethyl-phenyl-silanyl)-oct-7-en-3-one O-methyl-oxime

Guidance literature:: Multi-step reaction with 6 steps

1: Ni(acac)2 / tetrahydrofuran / 20 h / -20 °C

2: K₃Fe(CN)6; K₂CO₃; potassium osmium dihydrate / (DHQD)2PYR; methanesulfonamide / 2-methyl-propan-2-ol; H₂O / 30 h / 20 °C

3: 6.60 g / sodium periodate / methanol; tetrahydrofuran; H₂O / 1.5 h / 20 °C

4: tetrahydrofuran / 1 h / 0 °C

5: Dess-Martin periodinane / CH₂Cl₂ / 1 h / 20 °C

6: 0.266 g / sodium acetate / ethanol; H₂O / 2 h / 60 °C

With bis(acetylacetonate)nickel(II); sodium periodate; potassium osmium dihydrate; sodium acetate; potassium carbonate; Dess-Martin periodane; potassium hexacyanoferrate(III); hydroquinindine-2,5-diphenyl-4,6-pyrimidinediyl diether; methanesulfonamide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol061914e

Reference yield:

: 607732-69-4
Dimethyl-phenyl-((E)-6-phenyl-1-vinyl-hex-4-enyl)-silane

: 914928-09-9
6-(dimethyl-phenyl-silanyl)-oct-7-en-3-one O-methyl-oxime

Guidance literature:: Multi-step reaction with 5 steps

1: K₃Fe(CN)6; K₂CO₃; potassium osmium dihydrate / (DHQD)2PYR; methanesulfonamide / 2-methyl-propan-2-ol; H₂O / 30 h / 20 °C

2: 6.60 g / sodium periodate / methanol; tetrahydrofuran; H₂O / 1.5 h / 20 °C

3: tetrahydrofuran / 1 h / 0 °C

4: Dess-Martin periodinane / CH₂Cl₂ / 1 h / 20 °C

5: 0.266 g / sodium acetate / ethanol; H₂O / 2 h / 60 °C

With sodium periodate; potassium osmium dihydrate; sodium acetate; potassium carbonate; Dess-Martin periodane; potassium hexacyanoferrate(III); hydroquinindine-2,5-diphenyl-4,6-pyrimidinediyl diether; methanesulfonamide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol061914e