1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-2-[(4-methoxyphenyl)methyl]-6-[4-(trimethylsilyl)-3-butyn-1-yl ]-4-[(trimethylsilyl)oxy]-, phenyl ester

Base Information

Chemical Name:1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-2-[(4-methoxyphenyl)methyl]-6-[4-(trimethylsilyl)-3-butyn-1-yl ]-4-[(trimethylsilyl)oxy]-, phenyl ester
CAS No.:917879-26-6
Molecular Formula:C30H41NO4Si2
Molecular Weight:535.831
Hs Code.:

1(2H)-Pyridinecarboxylic acid,
3,6-dihydro-2-[(4-methoxyphenyl)methyl]-6-[4-(trimethylsilyl)-3-butyn-1-yl
]-4-[(trimethylsilyl)oxy]-, phenyl ester

Synonyms:

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Chemical Property of 1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-2-[(4-methoxyphenyl)methyl]-6-[4-(trimethylsilyl)-3-butyn-1-yl ]-4-[(trimethylsilyl)oxy]-, phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-2-[(4-methoxyphenyl)methyl]-6-[4-(trimethylsilyl)-3-butyn-1-yl ]-4-[(trimethylsilyl)oxy]-, phenyl ester

There total 4 articles about 1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-2-[(4-methoxyphenyl)methyl]-6-[4-(trimethylsilyl)-3-butyn-1-yl ]-4-[(trimethylsilyl)oxy]-, phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917879-06-2
2-(4-methoxybenzyl)-4-oxo-3,4-dihydro-2H-pyridine-1-carboxylic acid phenyl ester

: 75-77-4
chloro-trimethyl-silane

: 69361-41-7
4-bromo-1-trimethylsilylbut-1-yne

: 917879-26-6
2-(4-methoxy-benzyl)-6-(4-trimethylsilanyl-but-3-ynyl)-4-trimethylsilanyloxy-3,6-dihydro-2H-pyridine-1-carboxylic acid phenyl ester

Guidance literature:: 4-bromo-1-trimethylsilylbut-1-yne; With magnesium; In diethyl ether; at 10 - 20 ℃;

2-(4-methoxybenzyl)-4-oxo-3,4-dihydro-2H-pyridine-1-carboxylic acid phenyl ester; chloro-trimethyl-silane; With copper(I) bromide dimethylsulfide complex; triethylamine; In tetrahydrofuran;

In tetrahydrofuran; diethyl ether; at -78 - -45 ℃;
DOI:10.1021/jo061677t

Reference yield:

: 620-08-6,1232006-56-2
4-methoxypyridine

: 917879-26-6
2-(4-methoxy-benzyl)-6-(4-trimethylsilanyl-but-3-ynyl)-4-trimethylsilanyloxy-3,6-dihydro-2H-pyridine-1-carboxylic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: -78 °C

2.1: Mg / diethyl ether / 10 - 20 °C

2.2: CuBr*Me₂S; Et₃N / tetrahydrofuran

2.3: tetrahydrofuran; diethyl ether / -78 - -45 °C

With magnesium; In diethyl ether;
DOI:10.1021/jo061677t

Reference yield:

: 1885-14-9
phenyl chloroformate

: 917879-26-6
2-(4-methoxy-benzyl)-6-(4-trimethylsilanyl-but-3-ynyl)-4-trimethylsilanyloxy-3,6-dihydro-2H-pyridine-1-carboxylic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: -78 °C

2.1: Mg / diethyl ether / 10 - 20 °C

2.2: CuBr*Me₂S; Et₃N / tetrahydrofuran

2.3: tetrahydrofuran; diethyl ether / -78 - -45 °C

With magnesium; In diethyl ether;
DOI:10.1021/jo061677t