4-Nitro-N-[2-(prop-1-en-2-yl)phenyl]benzene-1-sulfonamide

Base Information

Chemical Name:4-Nitro-N-[2-(prop-1-en-2-yl)phenyl]benzene-1-sulfonamide
CAS No.:918297-95-7
Molecular Formula:C15H14N2O4S
Molecular Weight:318.353
Hs Code.:
DSSTox Substance ID:DTXSID90580260
Wikidata:Q82471041

Synonyms:918297-95-7;DTXSID90580260;4-Nitro-N-[2-(prop-1-en-2-yl)phenyl]benzene-1-sulfonamide

Suppliers and Price of 4-Nitro-N-[2-(prop-1-en-2-yl)phenyl]benzene-1-sulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4-Nitro-N-[2-(prop-1-en-2-yl)phenyl]benzene-1-sulfonamide

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:318.06742811
Heavy Atom Count:22
Complexity:513

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C)C1=CC=CC=C1NS(=O)(=O)C2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of 4-Nitro-N-[2-(prop-1-en-2-yl)phenyl]benzene-1-sulfonamide

There total 4 articles about 4-Nitro-N-[2-(prop-1-en-2-yl)phenyl]benzene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 52562-19-3
2-isopropenylaniline

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 918297-95-7
3-nitro-4-((2-(prop-1-en-2-yl)phenyl)amino)benzenesulfonic acid

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1055/s-0034-1379015

Reference yield:

: 551-93-9
2-aminoacetophenone

: 918297-95-7
3-nitro-4-((2-(prop-1-en-2-yl)phenyl)amino)benzenesulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.67 h / 0 - 20 °C

1.2: 0 - 20 °C

2.1: pyridine / dichloromethane / 20 °C / Inert atmosphere

With pyridine; potassium tert-butylate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.0c01823

Reference yield:

: C₈H₁₀N₂

: 918297-95-7
3-nitro-4-((2-(prop-1-en-2-yl)phenyl)amino)benzenesulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 0 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0.67 h / 0 - 20 °C

2.2: 0 - 20 °C

3.1: pyridine / dichloromethane / 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; potassium tert-butylate; water; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.0c01823