Benzoic acid, 3-ethenyl-4-(1-methylethoxy)-, methyl ester

Base Information

Chemical Name:Benzoic acid, 3-ethenyl-4-(1-methylethoxy)-, methyl ester
CAS No.:918870-83-4
Molecular Formula:C13H16O3
Molecular Weight:220.268
Hs Code.:

Synonyms:methyl 4-isopropoxy-3-vinylbenzoate;Benzoic acid,3-ethenyl-4-(1-methylethoxy)-,methyl ester;4-Isopropoxy-3-vinyl-benzoic acid methyl ester;

Suppliers and Price of Benzoic acid, 3-ethenyl-4-(1-methylethoxy)-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Benzoic acid, 3-ethenyl-4-(1-methylethoxy)-, methyl ester

Chemical Property:

Boiling Point:329.5±30.0 °C(Predicted)
PSA：35.53000
Density:1.045±0.06 g/cm3(Predicted)
LogP:2.90340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 3-ethenyl-4-(1-methylethoxy)-, methyl ester

There total 3 articles about Benzoic acid, 3-ethenyl-4-(1-methylethoxy)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 190271-78-4
methyl 3-formyl-4-isopropoxy-benzoate

: 1779-49-3
Methyltriphenylphosphonium bromide

: 918870-83-4
methyl 4-isopropoxy-3-vinylbenzoate

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium hexamethylsilazane; In toluene; for 1.5h;

methyl 3-formyl-4-isopropoxy-benzoate; In toluene; at -78 - 20 ℃; for 1.5h;
DOI:10.1002/chem.201100300

Reference yield: 56.0%

: 918870-83-4
methyl 4-isopropoxy-3-vinylbenzoate

Guidance literature:

Reference yield:

: 24589-99-9
methyl 3-formyl-4-hydroxybenzoate

: 918870-83-4
methyl 4-isopropoxy-3-vinylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; caesium carbonate / N,N-dimethyl-formamide / 7 h / 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / toluene / 1.5 h

2.2: 1.5 h / -78 - 20 °C

With potassium hexamethylsilazane; potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.201100300