2-IODO-1H,1H,2H,3H,3H-PERFLUORONONAN-1-OL

Base Information

• Chemical Name: 2-IODO-1H,1H,2H,3H,3H-PERFLUORONONAN-1-OL
• CAS No.: 38550-44-6
• Molecular Formula: C9H6 F13 I O
• Molecular Weight: 504.03
• Hs Code.: 2905590090
• Mol file: 38550-44-6.mol

Synonyms:2-Iodo-4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononan-1-ol;4,4,5,5,6,6,7,7,8,8,9,9,9-Tridecafluoro-2-iodo-1-nonanol

Chemical Property of 2-IODO-1H,1H,2H,3H,3H-PERFLUORONONAN-1-OL

Chemical Property:

• Vapor Pressure: 0.0305mmHg at 25°C
• Melting Point: 45oC
• Boiling Point: 216.3°Cat760mmHg
• Flash Point: 84.6°C
• PSA: 20.23000
• Density: 1.902g/cm³
• LogP: 4.91120

Purity/Quality:

98%min ^*data from raw suppliers

2-Iodo-1H,1H,2H,3H,3H-perfluorononan-1-ol ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-IODO-1H,1H,2H,3H,3H-PERFLUORONONAN-1-OL

There total 1 articles about 2-IODO-1H,1H,2H,3H,3H-PERFLUORONONAN-1-OL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

tris(allyl)borate (1693-71-6) + n-perfluorohexyl iodide (355-43-1) → 4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-1-iodononan-1-ol (38550-44-6) + allyl alcohol (107-18-6)

Guidance literature:

tris(allyl)borate; n-perfluorohexyl iodide; With 2,2'-azobis(isobutyronitrile); at 60 - 70 ℃; for 3h;

With water; at 60 ℃;

Reference yield: 90.0%

4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-1-iodononan-1-ol (38550-44-6) → 4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononan-1-ol (80806-68-4)

Guidance literature:

With tri-n-butyl-tin hydride; In toluene; at 20 ℃; for 12h;

DOI:10.1016/S0022-1139(00)00343-2

Reference yield: 81.0%

4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-1-iodononan-1-ol (38550-44-6) → 2-(2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoroheptyl)oxirane (38565-52-5)

Guidance literature:

With potassium hydroxide; In methanol; water; at 6 ℃; for 3h;

upstream raw materials:

tris(allyl)borate

n-perfluorohexyl iodide

Downstream raw materials:

2-(2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoroheptyl)oxirane

4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononan-1-ol

3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctanoic acid

2-Hydroxy-3-perfluorohexylpropanoic acid