Carbamic acid,[(1S)-1-[[(4S,5R)-5-hydroxy- 4-(phenylmethyl)-3-oxazolidinyl]carbonyl]-2- methylpropyl]-,phenylmethyl ester

Base Information

Chemical Name:Carbamic acid,[(1S)-1-[[(4S,5R)-5-hydroxy- 4-(phenylmethyl)-3-oxazolidinyl]carbonyl]-2- methylpropyl]-,phenylmethyl ester
CAS No.:180799-56-8
Molecular Formula:C₂₃H₂₈N₂O₅
Molecular Weight:412.486
Hs Code.:
Mol file:180799-56-8.mol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid,[(1S)-1-[[(4S,5R)-5-hydroxy- 4-(phenylmethyl)-3-oxazolidinyl]carbonyl]-2- methylpropyl]-,phenylmethyl ester

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Technology Process of Carbamic acid,[(1S)-1-[[(4S,5R)-5-hydroxy- 4-(phenylmethyl)-3-oxazolidinyl]carbonyl]-2- methylpropyl]-,phenylmethyl ester

There total 2 articles about Carbamic acid,[(1S)-1-[[(4S,5R)-5-hydroxy- 4-(phenylmethyl)-3-oxazolidinyl]carbonyl]-2- methylpropyl]-,phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 180799-66-0
[(S)-1-((S)-4-Benzyl-5-oxo-oxazolidine-3-carbonyl)-2-methyl-propyl]-carbamic acid benzyl ester

: 180799-56-8
MDL 104903

Guidance literature:: With diisobutylaluminium hydride; In toluene; at -78 ℃;
DOI:10.1016/S0960-894X(99)00391-1

Reference yield:

: 19542-51-9
N-benzyloxycarbonyl-L-valyl-L-phenylalanine

: 180799-56-8
MDL 104903

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / p-TsOH / benzene

2: 33 percent / diisobutylaluminum hydride / toluene / -78 °C

With diisobutylaluminium hydride; toluene-4-sulfonic acid; In toluene; benzene;
DOI:10.1016/S0960-894X(99)00391-1