Benzenecarbothioamide, 4-bromo-N-methyl-

Base Information

• Chemical Name: Benzenecarbothioamide, 4-bromo-N-methyl-
• CAS No.: 920510-22-1
• Molecular Formula: C8H8BrNS
• Molecular Weight: 230.12500
• Mol file: 920510-22-1.mol

Synonyms:Benzenecarbothioamide,4-bromo-N-methyl;

Chemical Property of Benzenecarbothioamide, 4-bromo-N-methyl-

Chemical Property:

• Melting Point: 135-136 °C(Solv: isopropanol (67-63-0))
• Boiling Point: 274.0±42.0 °C(Predicted)
• PSA: 44.12000
• Density: 1.495±0.06 g/cm3(Predicted)
• LogP: 2.73490

Purity/Quality:

99%, ^*data from raw suppliers

4-?Bromo-?N-?methylbenzothioamide 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenecarbothioamide, 4-bromo-N-methyl-

There total 1 articles about Benzenecarbothioamide, 4-bromo-N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-bromobenzenecarbonitrile (623-00-7) + methylamine (74-89-5) → C8H8BrNS (920510-22-1)

Guidance literature:

4-bromobenzenecarbonitrile; With diammonium sulfide; 1,6-bis(3-methylimidazolium-1-yl)hexane dichloride; at 70 ℃; for 0.0666667h;

methylamine; at 70 ℃; for 0.166667h;

DOI:10.1007/BF03246065

Reference yield: 79.0%

C8H8BrNS (920510-22-1) → 4-bromo-N-methylbenzamide (27466-83-7)

Guidance literature:

With tert.-butylhydroperoxide; copper(I) bromide; In 1,2-dichloro-ethane; at 50 ℃; for 3h;

DOI:10.3184/174751912X13318177149710

upstream raw materials:

4-bromobenzenecarbonitrile

methylamine

Downstream raw materials:

4-bromo-N-methylbenzamide