1-[4-(2-Phenylhydrazinyl)phenyl]ethanone

Base Information

Chemical Name:1-[4-(2-Phenylhydrazinyl)phenyl]ethanone
CAS No.:6311-55-3
Molecular Formula:C14H14N2O
Molecular Weight:226.278
Hs Code.:
NSC Number:43221
DSSTox Substance ID:DTXSID00285911
Wikidata:Q82021454

Synonyms:1-[4-(2-phenylhydrazinyl)phenyl]ethanone;6311-55-3;NSC43221;SCHEMBL16318184;DTXSID00285911;NSC-43221

Suppliers and Price of 1-[4-(2-Phenylhydrazinyl)phenyl]ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1-[4-(2-Phenylhydrazinyl)phenyl]ethanone

Chemical Property:

Vapor Pressure:0.0006mmHg at 25°C
Boiling Point:310.4°Cat760mmHg
Flash Point:111.4°C
Density:1.205g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:226.110613074
Heavy Atom Count:17
Complexity:241

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)C1=CC=C(C=C1)NNC2=CC=CC=C2

Technology Process of 1-[4-(2-Phenylhydrazinyl)phenyl]ethanone

There total 3 articles about 1-[4-(2-Phenylhydrazinyl)phenyl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 4827-16-1
4-acetoazobenzene

: 6311-55-3
1-<4-(2-phenylhydrazino)phenyl>ethanone

Guidance literature:: With tri-n-butyl-tin hydride; In benzene; for 2h; Heating;
DOI:10.1021/jo00028a038

Reference yield:

: 99-92-3
p-aminobenzophenone

: 98-95-3,26969-40-4
nitrobenzene

: 6311-55-3
1-<4-(2-phenylhydrazino)phenyl>ethanone

Guidance literature:: p-aminobenzophenone; nitrobenzene; With acetic acid; In ethanol; at 40 ℃; for 12h;

With ammonium chloride; zinc; In water; acetone; at 20 ℃; for 5h;
DOI:10.1039/c9gc00515c

Reference yield:

: 99-92-3
p-aminobenzophenone

: 586-96-9
Nitrosobenzene

: 6311-55-3
1-<4-(2-phenylhydrazino)phenyl>ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 20 °C / Cooling

2: ammonium chloride; zinc / water; acetone / 0 °C / Inert atmosphere

With ammonium chloride; acetic acid; zinc; In water; acetone;
DOI:10.1016/j.tet.2016.03.103