Benzene, [3-(ethenyloxy)-1-propenyl]-

Base Information

• Chemical Name: Benzene, [3-(ethenyloxy)-1-propenyl]-
• CAS No.: 940-52-3
• Molecular Formula: C11H12O
• Molecular Weight: 160.216
• Mol file: 940-52-3.mol

Synonyms:((Z)-3-Vinyloxy-propenyl)-benzene;Vinyl-γ-phenylallyl-ether;trans-Cinnamyl-vinyl-ether;Cinnamyl-vinyl-ether;

Chemical Property of Benzene, [3-(ethenyloxy)-1-propenyl]-

Chemical Property:

• PSA: 9.23000
• LogP: 2.85990

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzene, [3-(ethenyloxy)-1-propenyl]-

There total 5 articles about Benzene, [3-(ethenyloxy)-1-propenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-epoxy-3-phenylpropane (4436-24-2) + calcium carbide (75-20-7) → 3-phenyl-2-propenyl vinyl ether (940-52-3)

Guidance literature:

With caesium carbonate; In water; dimethyl sulfoxide; at 100 ℃; for 16h; Inert atmosphere; Sealed tube;

DOI:10.1002/cssc.201701153

Reference yield:

<β-Chlor-ethyl>-γ-chlor-γ-phenyl-propylether (13975-26-3) → 3-phenyl-2-propenyl vinyl ether (940-52-3)

Guidance literature:

With potassium hydroxide; In isopropyl alcohol;

Reference yield:

β-styrylmagnesium bromide (30094-01-0,35672-47-0,56516-81-5) → 3-phenyl-2-propenyl vinyl ether (940-52-3)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: KOtBu

With potassium tert-butylate; In tetrahydrofuran;

upstream raw materials:

(2-Brom-ethyl)-cinnamyl-ether

<β-Chlor-ethyl>-γ-chlor-γ-phenyl-propylether

cinnamic alcohol

ethyl vinyl ether

Downstream raw materials:

3-Phenylpentanal

3-phenylpentanoic acid

3-phenylpent-4-enoic acid

N-(3-phenyl-4-pentylidene)-2-benzothiazolesulfenamide