2,6-Dichloro-4-methoxybenzoic acid

Base Information

Chemical Name:2,6-Dichloro-4-methoxybenzoic acid
CAS No.:94278-69-0
Molecular Formula:C8H6Cl2O3
Molecular Weight:221.04
Hs Code.:
DSSTox Substance ID:DTXSID801298307

Synonyms:2,6-dichloro-4-methoxybenzoic acid;94278-69-0;2,6-dichloro-4-methoxy-benzoic acid;Benzoic acid, 2,6-dichloro-4-methoxy-;SCHEMBL596707;TYMXOVAJNLGZQC-UHFFFAOYSA-N;DTXSID801298307;AKOS023772785;F85679

Suppliers and Price of 2,6-Dichloro-4-methoxybenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,6-Dichloro-4-methoxybenzoic acid

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:219.9693994
Heavy Atom Count:13
Complexity:186

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C(=C1)Cl)C(=O)O)Cl

Technology Process of 2,6-Dichloro-4-methoxybenzoic acid

There total 3 articles about 2,6-Dichloro-4-methoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 86111-47-9
(2,6-dichloro-4-methoxy-phenyl)-methanol

: 94278-69-0
2,6-dichloro-4-methoxybenzoic acid

Guidance literature:: With tetra-n-butylammonium permanganate; In pyridine; at 100 ℃; for 1h;
DOI:10.1002/ardp.19903230204

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 33719-74-3
3,5-dichloroanisole

: 94278-69-0
2,6-dichloro-4-methoxybenzoic acid

: 94294-09-4
2,4-dichloro-6-methoxybenzoic acid

Guidance literature:: 3,5-dichloroanisole; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h; Inert atmosphere;

carbon dioxide;

With hydrogenchloride; In water; at 0 ℃; Overall yield = 57 %; Overall yield = 3.5 g;
DOI:10.1021/jm400266t