Stannane, trimethyl-2-naphthalenyl-

Base Information

Chemical Name:Stannane, trimethyl-2-naphthalenyl-
CAS No.:945-77-7
Molecular Formula:C13H16Sn
Molecular Weight:290.98
Hs Code.:2931900090
Mol file:945-77-7.mol

Synonyms:Trimethyl(2-naphthyl)stannane;(2-naphthyl)trimethylstannane;Stannane,trimethyl-2-naphthyl;2-trimethylstannylnaphthalene;Stannane,trimethyl-2-naphthalenyl;Naphth-2-yltrimethylstannane;

Suppliers and Price of Stannane, trimethyl-2-naphthalenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Stannane, trimethyl-2-naphthalenyl-

Chemical Property:

PSA：0.00000
LogP:2.89360

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Stannane, trimethyl-2-naphthalenyl-

There total 8 articles about Stannane, trimethyl-2-naphthalenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 16519-26-9
diethyl naphthalen-2-yl phosphate

: 1066-45-1
trimethyltin(IV)chloride

: 945-77-7
β-naphthyltrimethylstannane

Guidance literature:: With sodium; In ammonia; Irradiation (UV/VIS); (CH3)3SnCl was dissolved in ammonia, Na metal was added until a blue color persisted for 5 min, when the blue color dissapeared, phosphate esterwas added, the mixt. was UV-irradiated with stirring for 1 h; excess of CH3I was added, NH3 was evapd., the residue was treated with water, extd. with ether, washed with aq. satd. soln. of NaCl, dried over MgSO4, recrystd. in ethanol;
DOI:10.1021/om010878e

Reference yield: 95.6%

: 1336-21-6
ammonium hydroxide

: 580-13-2
2-bromonaphthalene

: 1066-45-1
trimethyltin(IV)chloride

: 594-19-4
tert.-butyl lithium

: 944-85-4
1-(trimethylstannyl)naphthalene

: 945-77-7
β-naphthyltrimethylstannane

Guidance literature:: In 1,4-dioxane; diethyl ether; pentane;

Reference yield: 89.0%

: 37827-83-1
naphthalene-2-carbonyl fluoride

: 661-69-8
hexamethyldistannane

: 945-77-7
β-naphthyltrimethylstannane

Guidance literature:: With 1,4-bis(dicyclohexylphosphino)butane; palladium dichloride; In o-xylene; at 140 ℃; for 10h; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.201901223