Diazene, dibenzoyl-

Base Information

• Chemical Name: Diazene, dibenzoyl-
• CAS No.: 959-31-9
• Molecular Formula: C14H10N2O2
• Molecular Weight: 238.246
• DSSTox Substance ID: DTXSID50449728
• Nikkaji Number: J60.350C
• Mol file: 959-31-9.mol

Synonyms:Diazene, dibenzoyl-;dibenzoyldiazene;Diimide, dibenzoyl-;959-31-9;Azobis(phenylmethanone);DTXSID50449728;STK330523;(E)-diazene-1,2-diylbis(phenylmethanone)

Chemical Property of Diazene, dibenzoyl-

Chemical Property:

• XLogP3: 3.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 238.074227566
• Heavy Atom Count: 18
• Complexity: 295

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)N=NC(=O)C2=CC=CC=C2

Technology Process of Diazene, dibenzoyl-

There total 12 articles about Diazene, dibenzoyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

benzoyl azide (582-61-6) → 1,2-dibenzoyldiazene (959-31-9)

Guidance literature:

With {[Cl₂NN]Cu}₂(μ-benzene); In benzene; Reagent/catalyst;

DOI:10.1002/anie.201810556

Reference yield: 19.0%

N-methoxybenzamide (2446-51-7) → 1,2-dibenzoyldiazene (959-31-9)

Guidance literature:

With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; boric acid; potassium hydrogencarbonate; In dichloromethane; at 90 ℃; for 24h; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.orglett.9b03357

Reference yield:

benzoic acid hydrazide (613-94-5) → 1,2-dibenzoyldiazene (959-31-9) + N'-benzoylbenzohydrazide (787-84-8)

Guidance literature:

With alkaline sodium hypochlorite; acetic acid;

upstream raw materials:

benzoic acid hydrazide

N'-benzoylbenzohydrazide

acetic acid

benzoyl chloride

Downstream raw materials:

tribenzoylhydrazine

2,5-bis-(phenyl)-1,3,4-oxadiazole

N,N'-dibenzoyl-N-(4-dimethylamino-phenyl)-hydrazine

2-benzhydrylidene-3-benzoyl-6,6,7a-triphenyl-dihydro-oxazolo[2,3-b][1,3,4]oxadiazol-5-one