2,3-Dichloro-2-methylpropionaldehyde

Base Information

• Chemical Name: 2,3-Dichloro-2-methylpropionaldehyde
• CAS No.: 10141-22-7
• Molecular Formula: C4H6 Cl2 O
• Molecular Weight: 140.997
• UNII: B389UMY29K
• DSSTox Substance ID: DTXSID90906148
• Nikkaji Number: J35.359K
• Wikidata: Q27274302
• Mol file: 10141-22-7.mol

Synonyms:2,3-dichloro-2-methylpropanal;2,3-Dichloro-2-methylpropionaldehyde;Propionaldehyde, 2,3-dichloro-2-methyl-;BRN 1745370;10141-22-7;Propanal, 2,3-dichloro-2-methyl-;UNII-B389UMY29K;B389UMY29K;4-01-00-03267 (Beilstein Handbook Reference);SCHEMBL6561359;2,3-Dichloro-2-methyl-propanal;DTXSID90906148;HWRRRIKZPDRSFG-UHFFFAOYSA-N;AKOS006387335;2,3-Dichloro-2-methyl propionaldehyde;LS-123974;Q27274302

Chemical Property of 2,3-Dichloro-2-methylpropionaldehyde

Chemical Property:

• Vapor Pressure: 1.86mmHg at 25°C
• Boiling Point: 165.6°Cat760mmHg
• Flash Point: 60.8°C
• Density: 1.229g/cm³
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 139.9795702
• Heavy Atom Count: 7
• Complexity: 74.1

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(CCl)(C=O)Cl

Technology Process of 2,3-Dichloro-2-methylpropionaldehyde

There total 1 articles about 2,3-Dichloro-2-methylpropionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-propan-1-ol (78-83-1) + chlorine (7782-50-5) → 2-chloroisobutyraldehyde (917-93-1) + 2-methyl-2,3-dichloropropionaldehyde (10141-22-7) + α-chloro-isobutyric acid isobutyl ester + α,β-dichloro-isobutyric acid isobutyl ester (19319-06-3)

Guidance literature:

Produkt 5-10:CO,CO₂,CH₃Cl,Isobuttersaeure,Oxyisobuttersaeure,Methacrylsaeure;

Reference yield: 78.0%

2-methyl-2,3-dichloropropionaldehyde (10141-22-7) + cyclohexylamine (108-91-8,157973-60-9) → N-(2,3-dichloro-2-methylpropylidene)cyclohexylamine (1331739-17-3)

Guidance literature:

With magnesium sulfate; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.tetlet.2011.06.062

upstream raw materials:

2-methyl-propan-1-ol

chlorine

Downstream raw materials:

N-(2,3-dichloro-2-methylpropylidene)cyclohexylamine

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