Carbamic acid, (2-iodophenyl)-, ethyl ester

Base Information

Chemical Name:Carbamic acid, (2-iodophenyl)-, ethyl ester
CAS No.:98952-64-8
Molecular Formula:C9H10INO2
Molecular Weight:291.088
Hs Code.:
DSSTox Substance ID:DTXSID20455553
Nikkaji Number:J465.010G
Wikidata:Q82277616

Synonyms:Carbamic acid, (2-iodophenyl)-, ethyl ester;98952-64-8;SCHEMBL2090928;DTXSID20455553;2-Iodophenylcarbamic acid ethyl ester;AKOS008929348;N-(2-Iodo-phenyl)-carbamic acid ethyl ester;J-522937

Suppliers and Price of Carbamic acid, (2-iodophenyl)-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Carbamic acid, (2-iodophenyl)-, ethyl ester

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:290.97563
Heavy Atom Count:13
Complexity:175

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)NC1=CC=CC=C1I

Technology Process of Carbamic acid, (2-iodophenyl)-, ethyl ester

There total 4 articles about Carbamic acid, (2-iodophenyl)-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 615-43-0
2-iodophenylamine

: 541-41-3
chloroformic acid ethyl ester

: 98952-64-8
N-ethoxycarbonyl-2-iodoaniline

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 18h;
DOI:10.1039/c4ob02493a

Reference yield: 81.0%

: 101-99-5
N-carboethoxyaniline

: 98952-64-8
N-ethoxycarbonyl-2-iodoaniline

Guidance literature:: With N-iodo-succinimide; methanesulfonic acid; nickel(II) chloride hexahydrate; In water; at 20 ℃; for 5h; Reagent/catalyst; Solvent; Temperature; regioselective reaction; Sealed tube; Microwave irradiation; Green chemistry;
DOI:10.1055/s-0040-1705972

Reference yield:

: 64-17-5
ethanol

: 1202047-19-5
1-tert-butyl-1-isopropyl-3-phenylurea

: 98952-64-8
N-ethoxycarbonyl-2-iodoaniline

Guidance literature:: 1-tert-butyl-1-isopropyl-3-phenylurea; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; at 0 ℃; for 3h; Inert atmosphere;

ethanol; With iodine; In tetrahydrofuran; diethyl ether; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1021/ol101102y