Technology Process of Carbamic acid, (2-iodophenyl)-, ethyl ester
There total 4 articles about Carbamic acid, (2-iodophenyl)-, ethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
at 20 ℃;
for 18h;
DOI:10.1039/c4ob02493a
- Guidance literature:
-
With
N-iodo-succinimide; methanesulfonic acid; nickel(II) chloride hexahydrate;
In
water;
at 20 ℃;
for 5h;
Reagent/catalyst;
Solvent;
Temperature;
regioselective reaction;
Sealed tube;
Microwave irradiation;
Green chemistry;
DOI:10.1055/s-0040-1705972
- Guidance literature:
-
1-tert-butyl-1-isopropyl-3-phenylurea;
With
n-butyllithium; N,N,N,N,-tetramethylethylenediamine;
In
diethyl ether; hexane;
at 0 ℃;
for 3h;
Inert atmosphere;
ethanol;
With
iodine;
In
tetrahydrofuran; diethyl ether; hexane;
at -78 ℃;
Inert atmosphere;
DOI:10.1021/ol101102y
