1,1'-[(2-Nitro-1,4-phenylene)disulfonyl]dibenzene

Base Information

• Chemical Name: 1,1'-[(2-Nitro-1,4-phenylene)disulfonyl]dibenzene
• CAS No.: 70415-93-9
• Molecular Formula: C₁₈H₁₃NO₆S₂
• Molecular Weight: 403.436
• NSC Number: 196868
• DSSTox Substance ID: DTXSID30307933
• Wikidata: Q82055549
• Mol file: 70415-93-9.mol

Synonyms:70415-93-9;NSC196868;DTXSID30307933;NSC-196868;1,1'-[(2-Nitro-1,4-phenylene)disulfonyl]dibenzene

Chemical Property of 1,1'-[(2-Nitro-1,4-phenylene)disulfonyl]dibenzene

Chemical Property:

• Vapor Pressure: 2.14E-15mmHg at 25°C
• Boiling Point: 636.2°Cat760mmHg
• Flash Point: 338.6°C
• Density: 1.451g/cm³
• XLogP3: 3.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 4
• Exact Mass: 403.01842948
• Heavy Atom Count: 27
• Complexity: 719

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)S(=O)(=O)C2=CC(=C(C=C2)S(=O)(=O)C3=CC=CC=C3)[N+](=O)[O-]

Technology Process of 1,1'-[(2-Nitro-1,4-phenylene)disulfonyl]dibenzene

There total 12 articles about 1,1'-[(2-Nitro-1,4-phenylene)disulfonyl]dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Nitro-1,4-bis-phenylthiobenzol (67745-29-3) → 1,4-bis-benzenesulfonyl-2-nitro-benzene (70415-93-9)

Guidance literature:

With dihydrogen peroxide; acetic acid;

DOI:10.1021/jo01329a010

Reference yield:

sodium thiophenolate (930-69-8) → 1,4-bis-benzenesulfonyl-2-nitro-benzene (70415-93-9)

Guidance literature:

Multi-step reaction with 2 steps

2: aq. H₂O₂, AcOH

With dihydrogen peroxide; acetic acid;

DOI:10.1021/jo01329a010

Reference yield:

1-chloro-2,4-dinitro-benzene (97-00-7) → 1,4-bis-benzenesulfonyl-2-nitro-benzene (70415-93-9)

Guidance literature:

Multi-step reaction with 2 steps

2: aq. H₂O₂, AcOH

With dihydrogen peroxide; acetic acid;

DOI:10.1021/jo01329a010

upstream raw materials:

1-benzenesulfonyl-2,4-dinitro-benzene

sodium benzenesulfonate

ethylene glycol

2-nitro-4-(phenylsulfonyl)chlorobenzene

Downstream raw materials:

2-nitro-4-phenylsulfonylphenol

2-nitro-4-(phenylsulphonyl)aniline

2-nitro-4-(phenylsulfonyl)chlorobenzene

4-benzenesulfonyl-2-nitro-1-(toluene-4-sulfonyl)-benzene