Diazene, bis[4-(pentyloxy)phenyl]-, 1-oxide

Base Information

• Chemical Name: Diazene, bis[4-(pentyloxy)phenyl]-, 1-oxide
• CAS No.: 19482-05-4
• Molecular Formula: C₂₂H₃₀N₂O₃
• Molecular Weight: 370.492
• Hs Code.: 2927000090
• Mol file: 19482-05-4.mol

Synonyms:4,4'-Diamyloxyazoxybenzene;19482-05-4;Diazene, bis[4-(pentyloxy)phenyl]-, 1-oxide;4,4'-di-n-Amyloxyazoxybenzene;oxido-(4-pentoxyphenyl)-(4-pentoxyphenyl)iminoazanium;4,4'-Dipentyloxyazoxybenzene;4,4'-Bis(pentyloxy)azoxybenzol;SCHEMBL19460599;4,4'-Bis(pentyloxy)azoxybenzene;MFCD00041933;AKOS015839686;CS-0435411;D1093;FT-0761426;T70504;(Z)-1,2-bis(4-(pentyloxy)phenyl)diazene oxide;(Z)-1,2-Bis(4-(pentyloxy)phenyl)diazene 1-oxide;107266-21-7

Chemical Property of Diazene, bis[4-(pentyloxy)phenyl]-, 1-oxide

Chemical Property:

• Vapor Pressure: 5.79E-10mmHg at 25°C
• Refractive Index: 1.6300 (estimate)
• Boiling Point: 508.7°Cat760mmHg
• Flash Point: 261.4°C
• PSA: 59.57000
• Density: 1.04g/cm³
• LogP: 7.27350
• Solubility.: almost transparency in hot Methanol
• XLogP3: 6.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 12
• Exact Mass: 370.22564282
• Heavy Atom Count: 27
• Complexity: 400

Purity/Quality:

98% ^*data from raw suppliers

4,4'-Diamyloxyazoxybenzene >95.0%(N) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCCCCOC1=CC=C(C=C1)N=[N+](C2=CC=C(C=C2)OCCCCC)[O-]

Technology Process of Diazene, bis[4-(pentyloxy)phenyl]-, 1-oxide

There total 7 articles about Diazene, bis[4-(pentyloxy)phenyl]-, 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-nitro-4-(pentyloxy)benzene (63469-11-4) → 4,4'-bis(pentyloxy)azoxybenzene (19482-05-4,107266-21-7)

Guidance literature:

With bismuth; at 20 ℃; for 3h;

DOI:10.1021/jo0203645

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → 4,4'-bis(pentyloxy)azoxybenzene (19482-05-4,107266-21-7)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide

2: 82 percent / bismuth / 3 h / 20 °C

With bismuth; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jo0203645

Reference yield:

1-Bromopentane (110-53-2) → 4,4'-bis(pentyloxy)azoxybenzene (19482-05-4,107266-21-7)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide

2: 82 percent / bismuth / 3 h / 20 °C

With bismuth; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jo0203645

upstream raw materials:

1-nitro-4-(pentyloxy)benzene

4-nitro-phenol

1-Bromopentane

amyl iodide

Refernces