cyclohexa-2,5-diene-1,4-diylbis(trimethylsilane)

Base Information

• Chemical Name: cyclohexa-2,5-diene-1,4-diylbis(trimethylsilane)
• CAS No.: 54380-47-1
• Molecular Formula: C12H24 Si2
• Molecular Weight: 224.494

Synonyms:Silane,2,5-cyclohexadiene-1,4-diylbis[trimethyl-, trans- (9CI); trans-3,6-Bis(trimethylsilyl)cyclohexa-1,4-diene

Chemical Property of cyclohexa-2,5-diene-1,4-diylbis(trimethylsilane)

Chemical Property:

• Vapor Pressure: 0.048mmHg at 25°C
• Boiling Point: 244.2°Cat760mmHg
• Flash Point: 85°C
• Density: 0.83g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of cyclohexa-2,5-diene-1,4-diylbis(trimethylsilane)

There total 2 articles about cyclohexa-2,5-diene-1,4-diylbis(trimethylsilane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro-trimethyl-silane (75-77-4) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → trans-3,6-bis(trimethylsilyl)-1,4-cyclohexadiene (54380-47-1) + cis-3,6-bis(trimethylsilyl)-1,4-cyclohexadiene (54380-45-9)

Guidance literature:

With lithium; In tetrahydrofuran; for 8h; Yields of byproduct given;

Reference yield:

→ trans-3,6-bis(trimethylsilyl)-1,4-cyclohexadiene (54380-47-1)

Guidance literature:

1,4-Bis(trimethylsilyl)benzol, Elektrolyse;

Reference yield:

trans-3,6-bis(trimethylsilyl)-1,4-cyclohexadiene (54380-47-1) + Triphenylmethyltetrafluoroborat → trimethylsilyl fluoride (420-56-4) + trimethylphenylsilane (768-32-1) + triphenylmethane (519-73-3)

Guidance literature:

With iron pentacarbonyl; Product distribution; 1) Bu₂O, 150 deg C, 20 h, 2) CH₂Cl₂, 1 h, r.t.;

upstream raw materials:

chloro-trimethyl-silane

benzene

Downstream raw materials:

trimethylsilyl fluoride

trimethylphenylsilane

triphenylmethane

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