Soyasapogenol　D

Base Information

• Chemical Name: Soyasapogenol D
• CAS No.: 65892-76-4
• Molecular Formula: C31H52O3
• Molecular Weight: 472.752

Synonyms:21ξ-Methoxy-olean-13(18)-en-3β,24-diol;(4aR)-3t-Hydroxy-10ξ-methoxy-4c,6at,6bc,8at,11,11,14bt-heptamethyl-4t-hydroxymethyl-(4arH,14acH)-Δ12a-eicosahydro-picen;21ξ-Methoxy-oleanen-(13(18))-diol-(3β,24);

Chemical Property of Soyasapogenol　D

Chemical Property:

• Vapor Pressure: 3.74E-14mmHg at 25°C
• Boiling Point: 545.1°Cat760mmHg
• Flash Point: 283.4°C
• PSA: 49.69000
• Density: 1.07g/cm³
• LogP: 6.91030

Purity/Quality:

≥98% ^*data from raw suppliers

Soyasapogenol D ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Soyasapogenol　D

There total 3 articles about Soyasapogenol　D which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

soyasaponin I (51330-27-9) → D-glucuronic acid (489-91-8,528-16-5,552-12-5,577-46-8,643-33-4,2240-07-5,6294-16-2,10133-02-5,18402-78-3,18968-14-4,21179-08-8,23018-83-9,33599-45-0,33599-46-1,46171-67-9,46171-69-1,46172-26-3,70021-34-0,71031-08-8,104195-06-4,106499-29-0,124817-72-7) + L-rhamnose (6014-42-2) + β-D-galactopyranoside (7296-64-2) + 3β,24-dihydroxy-22β-methoxyolean-13(18)-en (65892-76-4) + soyasapogenol C (595-14-2) + soyasapogenol B (124862-79-9,595-15-3)

Guidance literature:

With hydrogenchloride; water; In methanol; at 80 ℃; for 3h;

DOI:10.1021/jf8036984

Reference yield:

methanol (67-56-1) + soyasaponin I (51330-27-9) → 3β,24-dihydroxy-22β-methoxyolean-13(18)-en (65892-76-4) + 3β,22β,24-trihydroxyolean-18(19)-en + 3β,22β,24-trihydroxyolean-13(18)-en + soyasapogenol C (595-14-2) + soyasapogenol B (124862-79-9,595-15-3)

Guidance literature:

With hydrogenchloride; In water; for 8h; Reflux;

DOI:10.1016/j.phytochem.2017.02.018

Reference yield:

→ 21ξ-methoxy-olean-13(18)-ene-3β,24-diol (65892-76-4)

Guidance literature:

With hydrogenchloride; anschliessendes Chromatographieren an Aluminiumoxyd;

DOI:10.1002/hlca.19580410713

upstream raw materials:

soyasaponin I

methanol

Downstream raw materials:

formaldehyd

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