Technology Process of Trinitroacetonitrile
There total 6 articles about Trinitroacetonitrile which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
cyanoacetic acid amide;
With
nitric acid;
In
tetrachloromethane;
at 0 ℃;
Inert atmosphere;
With
oleum, fuming sulfuric acid, 20% SO3;
In
tetrachloromethane;
at -20 - 20 ℃;
Inert atmosphere;
DOI:10.1021/ic400919n
- Guidance literature:
-
acetylcyanamide; nitric acid;
In
dichloromethane;
at 0 ℃;
for 0.0333333h;
Inert atmosphere;
With
sulfuric acid; sulfur trioxide;
In
dichloromethane;
at 25 ℃;
for 8 - 10h;
Inert atmosphere;
DOI:10.1039/c5dt00291e
- Guidance literature:
-
With
sulfuric acid; nitric acid;
