Benzonitrile,4-(benzoyloxy)-

Base Information

• Chemical Name: Benzonitrile,4-(benzoyloxy)-
• CAS No.: 16513-72-7
• Molecular Formula: C14H9 N O2
• Molecular Weight: 223.231
• Mol file: 16513-72-7.mol

Synonyms:Benzonitrile,p-hydroxy-, benzoate (ester) (8CI); 4-Cyanophenyl benzoate; p-Cyanophenylbenzoate

Chemical Property of Benzonitrile,4-(benzoyloxy)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzonitrile,4-(benzoyloxy)-

There total 32 articles about Benzonitrile,4-(benzoyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-cyanophenol (767-00-0) + benzoic acid anhydride (93-97-0) → 4-cyanophenyl benzoate (16513-72-7)

Guidance literature:

With magnesium(II) perchlorate; at 80 ℃; for 0.75h;

DOI:10.1016/j.tet.2003.08.007

Reference yield: 100.0%

4-cyanophenol (767-00-0) + 2,4-dinitrophenyl benzoate (1523-15-5) → 4-cyanophenyl benzoate (16513-72-7) + potassium 2,4-dinitrophenolate (14314-69-3)

Guidance literature:

With potassium hydrogencarbonate; In N,N-dimethyl-formamide; at 25 ℃; for 5h;

DOI:10.1134/S1070428011060030

Reference yield: 99.0%

4-cyanophenol (767-00-0) + benzaldehyde (100-52-7) → 4-cyanophenyl benzoate (16513-72-7)

Guidance literature:

With bis(2,6-diisopropylphenyl)-3,4,5,6-tetrahydropyrimidin-1-ium chloride; palladium diacetate; sodium carbonate; In 5,5-dimethyl-1,3-cyclohexadiene; at 100 ℃; for 24h; Sealed tube;

DOI:10.1016/j.tetlet.2011.03.017

upstream raw materials:

4-(benzoyloxy)benzoyl cyanide

4-cyanophenyl N-isopropylbenzimidate

4-cyanophenol

benzoic acid anhydride

Downstream raw materials:

benzoic acid ethyl ester

4-cyanophenolate

N-(N'-benzoyl-2-aminoethanoyl)-2-aminoethanoic acid

4-cyanophenol