3-Benzoyloxycholesta-8,14-diene

Base Information

Chemical Name:3-Benzoyloxycholesta-8,14-diene
CAS No.:20748-23-6
Molecular Formula:C34H48O2
Molecular Weight:488.7437
Hs Code.:
DSSTox Substance ID:DTXSID70942963
Mol file:20748-23-6.mol

Synonyms:3-benzoyloxycholesta-8,14-diene;3beta-benzoyloxy-5beta-cholesta-8,14-diene

Suppliers and Price of 3-Benzoyloxycholesta-8,14-diene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Benzoyloxycholesta-8,14-diene

Chemical Property:

Vapor Pressure:1.69E-13mmHg at 25°C
Boiling Point:581.1°Cat760mmHg
Flash Point:224.3°C
PSA：26.30000
Density:1.05g/cm³
LogP:9.31760
XLogP3:9.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:8
Exact Mass:488.365430770
Heavy Atom Count:36
Complexity:874

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)CCCC(C)C1CC=C2C1(CCC3=C2CCC4C3(CCC(C4)OC(=O)C5=CC=CC=C5)C)C
Isomeric SMILES:C[C@H](CCCC(C)C)[C@H]1CC=C2[C@@]1(CCC3=C2CCC4[C@@]3(CC[C@@H](C4)OC(=O)C5=CC=CC=C5)C)C

Technology Process of 3-Benzoyloxycholesta-8,14-diene

There total 8 articles about 3-Benzoyloxycholesta-8,14-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 19431-20-0
3β-hydroxy-5α-cholest-8,14-diene

: 98-88-4
benzoyl chloride

: 74524-23-5,20748-23-6
(3β,5α,17β)-colesta-8,14-dien-3-ol benzoate

Guidance literature:: With pyridine; at 90 ℃; for 1h;
DOI:10.1021/jo00243a021

Reference yield:

: 1182-06-5
3β-benzoyloxycholesta-5,7-diene

: 34227-12-8
(3β,5α)-cholesta-7,14-dien-3-ol benzoate

: 113349-58-9,20748-23-6
3β-(benzoyloxy)-5β-cholesta-8,14-diene

Guidance literature:: With hydrogenchloride; In dichloromethane; chloroform; at -70 ℃; Yields of byproduct given;
DOI:10.1021/jo00243a021

Reference yield:

: 1182-06-5
3β-benzoyloxycholesta-5,7-diene

: 74524-23-5,20748-23-6
Benzoic acid (3S,10S,13R,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,5,6,7,10,11,12,13,16,17-dodecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

: 34227-12-8
3b-hydroxycholesta-7,14-diene benzoate

Guidance literature:: With hydrogenchloride; In dichloromethane; at -40 - -30 ℃; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00371a025