4-chloro-N,N-dimethylbenzenecarbothioamide

Base Information

Chemical Name:4-chloro-N,N-dimethylbenzenecarbothioamide
CAS No.:15563-46-9
Molecular Formula:C9H10 Cl N S
Molecular Weight:199.704
Hs Code.:
NSC Number:202825
DSSTox Substance ID:DTXSID20308252
Nikkaji Number:J3.334.033H
Wikidata:Q82056035
Mol file:15563-46-9.mol

Synonyms:15563-46-9;4-chloro-N,N-dimethylbenzenecarbothioamide;NSC202825;DTXSID20308252;AKOS000349083;NSC-202825

Suppliers and Price of 4-chloro-N,N-dimethylbenzenecarbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 4-chloro-N,N-dimethylbenzenecarbothioamide

Chemical Property:

Vapor Pressure:0.0121mmHg at 25°C
Boiling Point:260.6°Cat760mmHg
Flash Point:111.4°C
Density:1.213g/cm³
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:199.0222482
Heavy Atom Count:12
Complexity:162

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C(=S)C1=CC=C(C=C1)Cl

Technology Process of 4-chloro-N,N-dimethylbenzenecarbothioamide

There total 13 articles about 4-chloro-N,N-dimethylbenzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 506-59-2
N,N-dimethylammonium chloride

: 104-88-1
4-chlorobenzaldehyde

: 15563-46-9
4-chloro-N,N-dimethylbenzenecarbothioamide

Guidance literature:: With sulfur; sodium acetate; In N,N-dimethyl-formamide; at 100 ℃; for 3h;
DOI:10.1055/s-1983-30490

Reference yield: 91.0%

: 14062-80-7
N,N-dimethyl-4-chlorobenzamide

: 15563-46-9
4-chloro-N,N-dimethylbenzenecarbothioamide

Guidance literature:: With diethyl dithiophosphate ammonium salt; In toluene; for 6h; Reflux;
DOI:10.1055/s-0031-1289859

Reference yield: 89.0%

: 104-88-1
4-chlorobenzaldehyde

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 15563-46-9
4-chloro-N,N-dimethylbenzenecarbothioamide

Guidance literature:: With sodiumsulfide nonahydrate; dibenzoyl peroxide; In water; at 100 ℃; for 12h; Schlenk technique;
DOI:10.1021/acs.orglett.5b03541