N,N-Diethylallylamine

Base Information

• Chemical Name: N,N-Diethylallylamine
• CAS No.: 5666-17-1
• Molecular Formula: C7H15N
• Molecular Weight: 113.203
• Hs Code.: 2921199090
• European Community (EC) Number: 679-708-2
• DSSTox Substance ID: DTXSID2063973
• Nikkaji Number: J150.877F
• Wikidata: Q81991138
• Mol file: 5666-17-1.mol

Synonyms:N,N-Diethylallylamine;5666-17-1;Allyldiethylamine;N,N-diethylprop-2-en-1-amine;diethylallylamine;N,N-Diethyl-2-propen-1-amine;N-Allyldiethylamine;2-Propen-1-amine, N,N-diethyl-;diethyl(prop-2-en-1-yl)amine;allyldiethyl amine;allyl diethyl amine;allyl-diethyl-amine;3-(Diethylamino)-1-propene;SCHEMBL251491;DTXSID2063973;SCHEMBL13123559;N,N-Diethyl-2-propen-1-amine #;ADAL1243001;MFCD00048537;AKOS006227951;BS-23701;CS-0204947;D1185;FT-0629466;D89806;A825295

Chemical Property of N,N-Diethylallylamine

Chemical Property:

• Vapor Pressure: 24.2mmHg at 25°C
• Refractive Index: 1.431
• Boiling Point: 110 °C at 760 mmHg
• PKA: 9.79±0.25(Predicted)
• Flash Point: 14 °C
• PSA: 3.24000
• Density: 0.773 g/cm³
• LogP: 1.51420
• XLogP3: 1.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 113.120449483
• Heavy Atom Count: 8
• Complexity: 55.4

Purity/Quality:

98%,99%, ^*data from raw suppliers

N,N-Diethylallylamine >98.0%(GC)(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C
• Hazard Codes: C

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)CC=C

Technology Process of N,N-Diethylallylamine

There total 20 articles about N,N-Diethylallylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

[Pd(η1-C3H5)(N,1-bis[2-(diphenylphosphino)phenyl]methanimine)]BF4 (1402556-62-0) + diethylamine (109-89-7) + 1,2-Dicyanoethylene (764-42-1) → N,N-diethylallylamine (5666-17-1) + [Pd(η2-fumaronitrile)(N,1-Bis[2-(diphenylphosphino)phenyl]methanimine)]·CH2Cl2

Guidance literature:

In chloroform-d1; at 24.84 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c2dt30746d

Reference yield: 41.6%

ethylamine (75-04-7,85404-22-4) + Allyl-but-2-ynyl-diethyl-ammonium; bromide (7796-61-4) → N,N-diethylallylamine (5666-17-1) + Allyl-[2-eth-(E)-ylidene-pent-4-en-(E)-ylidene]-amine (105379-94-0) + diethylamine (109-89-7)

Guidance literature:

With potassium hydroxide; at 90 - 95 ℃; for 5h;

Reference yield:

N,N-diethyl-2-propynylamine (4079-68-9,125678-52-6) → N,N-diethylpropylamine (4458-31-5) + N,N-diethylallylamine (5666-17-1)

Guidance literature:

With Ru(CH₉BBNMepi)PPh₃; hydrogen; In benzene-d6; at 80 ℃; for 2h; under 2311.54 Torr; Inert atmosphere; Schlenk technique;

DOI:10.1021/jacs.6b03972

upstream raw materials:

ethyl iodide

1-amino-2-propene

ethylamine

Allyl-but-2-ynyl-diethyl-ammonium; bromide

Downstream raw materials:

1-penten

diethylamino diethylaluminium

3-diethylaminopropyl chloride

1-diethylamino-2-chloropropane