1-(1-Bromonaphthalen-2-yl)-n,n-dimethylmethanamine

Base Information

Chemical Name:1-(1-Bromonaphthalen-2-yl)-n,n-dimethylmethanamine
CAS No.:15000-91-6
Molecular Formula:C13H14 Br N
Molecular Weight:264.161
Hs Code.:
NSC Number:100673
DSSTox Substance ID:DTXSID10933850
Wikidata:Q82909678
Mol file:15000-91-6.mol

Synonyms:15000-91-6;1-(1-bromonaphthalen-2-yl)-n,n-dimethylmethanamine;NSC100673;NCIOpen2_006883;DTXSID10933850;NSC-100673;1-bromo-2-(N,N-dimethylamino-methyl)naphthalene

Suppliers and Price of 1-(1-Bromonaphthalen-2-yl)-n,n-dimethylmethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-(1-Bromonaphthalen-2-yl)-n,n-dimethylmethanamine

Chemical Property:

Vapor Pressure:0.000193mmHg at 25°C
Boiling Point:328.2°Cat760mmHg
Flash Point:152.3°C
Density:1.345g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:263.03096
Heavy Atom Count:15
Complexity:205

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)CC1=C(C2=CC=CC=C2C=C1)Br

Technology Process of 1-(1-Bromonaphthalen-2-yl)-n,n-dimethylmethanamine

There total 2 articles about 1-(1-Bromonaphthalen-2-yl)-n,n-dimethylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 37763-43-2
1-bromo-2-(bromomethyl)naphthalene

: 124-40-3
dimethyl amine

: 15000-91-6
1-(1-bromonaphthalen-2-yl)-N,N-dimethylmethanamine

Guidance literature:: In ethanol; dichloromethane; for 18h; Reflux;
DOI:10.1002/anie.201811343

Reference yield:

: 2586-62-1
1-bromo-2-methylnaphtalene

: 15000-91-6
1-(1-bromonaphthalen-2-yl)-N,N-dimethylmethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: NBS / CCl₄ / Heating; Irradiation

With N-Bromosuccinimide; In tetrachloromethane;
DOI:10.1002/jps.2600510915

Reference yield: 95.0%

: 15000-91-6
1-(1-bromonaphthalen-2-yl)-N,N-dimethylmethanamine

: 87100-15-0
cyclohexylboronic acid pinacol ester

: 2-(1-cyclohexyl-2-methylene-1,2-dihydronaphthalen-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 1-(1-bromonaphthalen-2-yl)-N,N-dimethylmethanamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

cyclohexylboronic acid pinacol ester; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.5h;

With 2,2,2-trichloro-1,1-dimethylethoxychloroformate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.5h;
DOI:10.1002/anie.201811343