3,12-Epoxy-12H-pyrano[4,3-j]-1,2- benzodioxepin-10(3H)-one,octahydro-3,6- dimethyl-9-(3-phenylpropyl)-,(3R,5aS,6R,- 8aS,9R,12S,12aR)-

Base Information

Chemical Name:3,12-Epoxy-12H-pyrano[4,3-j]-1,2- benzodioxepin-10(3H)-one,octahydro-3,6- dimethyl-9-(3-phenylpropyl)-,(3R,5aS,6R,- 8aS,9R,12S,12aR)-
CAS No.:139727-68-7
Molecular Formula:C₂₃H₃₀O₅
Molecular Weight:386.488
Hs Code.:
Mol file:139727-68-7.mol

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Chemical Property of 3,12-Epoxy-12H-pyrano[4,3-j]-1,2- benzodioxepin-10(3H)-one,octahydro-3,6- dimethyl-9-(3-phenylpropyl)-,(3R,5aS,6R,- 8aS,9R,12S,12aR)-

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Technology Process of 3,12-Epoxy-12H-pyrano[4,3-j]-1,2- benzodioxepin-10(3H)-one,octahydro-3,6- dimethyl-9-(3-phenylpropyl)-,(3R,5aS,6R,- 8aS,9R,12S,12aR)-

There total 18 articles about 3,12-Epoxy-12H-pyrano[4,3-j]-1,2- benzodioxepin-10(3H)-one,octahydro-3,6- dimethyl-9-(3-phenylpropyl)-,(3R,5aS,6R,- 8aS,9R,12S,12aR)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 195060-82-3
(R)-2-((1R,4R,4aS,8aS)-4,7-Dimethyl-1,2,3,4,4a,5,6,8a-octahydro-naphthalen-1-yl)-5-phenyl-pentanoic acid

: 139727-68-7
JAV-146

Guidance literature:: With amberlyst-15; oxygen;
DOI:10.1016/S0040-4039(97)01428-7

Reference yield: 30.0%

: 17376-04-4
2-phenethyl iodide

: 101020-89-7
dehydroqinghaosu

: 139727-68-7
JAV-146

: 613233-56-0
(+)-octahydro-3,6α-dimethyl-3,12-epoxy-9α-(3'-phenylpropyl)-12H-pyrano [4,3j]-1,2-benzodioxepin-10(3H)-one

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 9h; Heating;
DOI:10.1021/jm030181q

Reference yield: 28.0%

: 139727-41-6
(1''S,1'''S,3''S,6''R)-(2''E)-2-<2'-<3''-(1'''-carboxy-4'''-phenylbutyl)-6''-methyl-2''-<(trimethylsilyl)methylene>cyclohexyl>ethyl>-2,5,5-trimethyl-1,3-dioxane

: 139727-68-7
JAV-146

Guidance literature:: (1''S,1'''S,3''S,6''R)-(2''E)-2-<2'-<3''-(1'''-carboxy-4'''-phenylbutyl)-6''-methyl-2''-<(trimethylsilyl)methylene>cyclohexyl>ethyl>-2,5,5-trimethyl-1,3-dioxane; With ozone; In dichloromethane; at -78 ℃; under 362.004 Torr;

With sulfuric acid; silica gel; In dichloromethane; at 20 ℃;
DOI:10.1021/jm020142z