6-[[2-[bis[2-[(3,5-dichloro-6-oxo-1-cyclohexa-2,4-dienylidene)methylamino]ethyl]amino]ethylamino]methylidene]-2,4-dichloro-cyclohexa-2,4-dien-1-one

Base Information

• Chemical Name: 6-[[2-[bis[2-[(3,5-dichloro-6-oxo-1-cyclohexa-2,4-dienylidene)methylamino]ethyl]amino]ethylamino]methylidene]-2,4-dichloro-cyclohexa-2,4-dien-1-one
• CAS No.: 70292-82-9
• Molecular Formula: C27H24Cl6N4O3
• Molecular Weight: 665.231

Synonyms:

Chemical Property of 6-[[2-[bis[2-[(3,5-dichloro-6-oxo-1-cyclohexa-2,4-dienylidene)methylamino]ethyl]amino]ethylamino]methylidene]-2,4-dichloro-cyclohexa-2,4-dien-1-one

Chemical Property:

• Boiling Point: 657.6°Cat760mmHg
• Flash Point: 351.5°C
• Density: 1.51g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-[[2-[bis[2-[(3,5-dichloro-6-oxo-1-cyclohexa-2,4-dienylidene)methylamino]ethyl]amino]ethylamino]methylidene]-2,4-dichloro-cyclohexa-2,4-dien-1-one

There total 2 articles about 6-[[2-[bis[2-[(3,5-dichloro-6-oxo-1-cyclohexa-2,4-dienylidene)methylamino]ethyl]amino]ethylamino]methylidene]-2,4-dichloro-cyclohexa-2,4-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2',2''-triaminotriethylamine (4097-89-6) + 3,5-dichlorosalicyclaldehyde (90-60-8) → tris{2-[(3,5-dichlorosalicylidene)amino]ethyl}amine (70292-82-9)

Guidance literature:

In ethanol; Heating;

DOI:10.1039/DT9910003259

Reference yield:

→ tris{2-[(3,5-dichlorosalicylidene)amino]ethyl}amine (70292-82-9)

Guidance literature:

entspr. Aldehyd, N(CH2CH2NH2)3 (in Ae.);

Reference yield: 72.0%

tetra-n-butylammonium permanganate (35638-41-6) + tris{2-[(3,5-dichlorosalicylidene)amino]ethyl}amine (70292-82-9) + manganese (II) acetate tetrahydrate (6156-78-1) → Mn(N(CH2CH2NCHC6H2(3,5-Cl2)O)3) (138497-36-6)

Guidance literature:

In ethanol; addn. of solid Mn(OAc)2*4H2O to a soln. of the ligand in hot ethanol; stirring at 330 K for 15 min; addn. of (NBu4)MnO4 in portions; stirring for 0.5 h;; removal of solvent under vac.; dissoln. in DMF; filtration; slow evapn. of filtrate at room temp.; the ppt. was filtered off and dried in air; recrystn. from DMF; elem. anal.;

DOI:10.1039/DT9910002917

upstream raw materials:

2,2',2''-triaminotriethylamine

3,5-dichlorosalicyclaldehyde

Downstream raw materials:

Co⁽³⁺⁾*(Cl₂OC₆H₂CHNCH₂CH₂)3N^(3-)=Co(Cl₂OC₆H₂CHNCH₂CH₂)3N

Mn(N(CH₂CH₂NCHC₆H₂(3,5-Cl₂)O)3)

Pr⁽³⁺⁾*(Cl₂OC₆H₂CHNCH₂CH₂)3N^(3-)=Pr(Cl₂OC₆H₂CHNCH₂CH₂)3N

Nd⁽³⁺⁾*(Cl₂OC₆H₂CHNCH₂CH₂)3N^(3-)=Nd(Cl₂OC₆H₂CHNCH₂CH₂)3N

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