Dimethylcarbamic acid 2-benzoylphenyl ester

Base Information

Chemical Name:Dimethylcarbamic acid 2-benzoylphenyl ester
CAS No.:74537-09-0
Molecular Formula:C16H15NO3
Molecular Weight:269.2952
Hs Code.:
DSSTox Substance ID:DTXSID30225542
Wikidata:Q83104545

Synonyms:Dimethylcarbamic acid 2-benzoylphenyl ester;74537-09-0;DTXSID30225542

Suppliers and Price of Dimethylcarbamic acid 2-benzoylphenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethylcarbamic acid 2-benzoylphenyl ester

Chemical Property:

Vapor Pressure:1.9E-07mmHg at 25°C
Boiling Point:425.6°Cat760mmHg
Flash Point:211.2°C
Density:1.176g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:269.10519334
Heavy Atom Count:20
Complexity:348

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C(=O)OC1=CC=CC=C1C(=O)C2=CC=CC=C2

Technology Process of Dimethylcarbamic acid 2-benzoylphenyl ester

There total 4 articles about Dimethylcarbamic acid 2-benzoylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 6969-90-0
phenyl N,N-dimethylcarbamate

: 611-73-4
Benzoylformic acid

: 74537-09-0
2-benzoylphenyl dimethylcarbamate

Guidance literature:: With ammonium peroxydisulfate; trifluorormethanesulfonic acid; palladium diacetate; In 1,2-dichloro-ethane; at 20 ℃; for 20h; Sealed tube;
DOI:10.1002/adsc.201200993

Reference yield:

: 6969-90-0
phenyl N,N-dimethylcarbamate

: 611-73-4
Benzoylformic acid

: 74537-09-0
2-benzoylphenyl dimethylcarbamate

: 1452841-54-1
2,6-dibenzoylphenyl dimethylcarbamate

Guidance literature:: With ammonium peroxydisulfate; trifluorormethanesulfonic acid; palladium diacetate; In 1,2-dichloro-ethane; at 20 ℃; for 20h; Reagent/catalyst; Concentration; Overall yield = 68 %; Sealed tube;
DOI:10.1002/adsc.201200993

Reference yield:

: 98-86-2
acetophenone

: 74537-09-0
2-benzoylphenyl dimethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: selenium(IV) oxide; pyridine

2: palladium diacetate; ammonium peroxydisulfate; trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 20 h / 20 °C / Sealed tube

With pyridine; selenium(IV) oxide; ammonium peroxydisulfate; trifluorormethanesulfonic acid; palladium diacetate; In 1,2-dichloro-ethane;
DOI:10.1002/adsc.201200993