Hydrazinecarbothioamide, N-(4-methylphenyl)-2-phenyl-

Base Information

Chemical Name:Hydrazinecarbothioamide, N-(4-methylphenyl)-2-phenyl-
CAS No.:22814-94-4
Molecular Formula:C14H15 N3 S
Molecular Weight:257.359
Hs Code.:
DSSTox Substance ID:DTXSID50409024
NSC Number:49343

Synonyms:22814-94-4;NSC49343;Hydrazinecarbothioamide, N-(4-methylphenyl)-2-phenyl-;DTXSID50409024;NSC-49343

Suppliers and Price of Hydrazinecarbothioamide, N-(4-methylphenyl)-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Hydrazinecarbothioamide, N-(4-methylphenyl)-2-phenyl-

Chemical Property:

Vapor Pressure:5.27E-06mmHg at 25°C
Boiling Point:380.9°Cat760mmHg
Flash Point:184.2°C
Density:1.268g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:257.09866866
Heavy Atom Count:18
Complexity:256

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)NC(=S)NNC2=CC=CC=C2

Technology Process of Hydrazinecarbothioamide, N-(4-methylphenyl)-2-phenyl-

There total 11 articles about Hydrazinecarbothioamide, N-(4-methylphenyl)-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-63-0
phenylhydrazine

: 622-59-3
1-isothiocyanato-4-methylbenzene

: 22814-94-4
N-(p-tolyl)-2-phenylhydrazinecarbothioamide

Guidance literature:: In toluene; at 20 ℃; for 1h;
DOI:10.1016/j.bioorg.2018.07.035

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 50878-38-1
methyl 2-phenylhydrazinecarbodithioate

: 22814-94-4
N-(p-tolyl)-2-phenylhydrazinecarbothioamide

Guidance literature:: With triethylamine; In 1,4-dioxane; at 100 ℃; for 4h;

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 22814-94-4
N-(p-tolyl)-2-phenylhydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water / 6 h / Reflux

2: chlorobenzene / 8 h / Reflux

3: 0.03 h / 20 °C

With hydrogenchloride; In water; chlorobenzene;
DOI:10.3390/molecules25112537