N-[1-[2-[(4-butoxy-3-ethoxyphenyl)methylidene]hydrazinyl]-3-methyl-1-oxobutan-2-yl]-3,4-dichlorobenzamide

Base Information

Chemical Name:N-[1-[2-[(4-butoxy-3-ethoxyphenyl)methylidene]hydrazinyl]-3-methyl-1-oxobutan-2-yl]-3,4-dichlorobenzamide
CAS No.:5856-22-4
Molecular Formula:C₁₀H₂₀O₆
Molecular Weight:236.265
Hs Code.:
DSSTox Substance ID:DTXSID40413817

Synonyms:5856-22-4;DTXSID40413817;N-(1-{2-[(4-Butoxy-3-ethoxyphenyl)methylidene]hydrazinyl}-3-methyl-1-oxobutan-2-yl)-3,4-dichlorobenzamide (non-preferred name)

Suppliers and Price of N-[1-[2-[(4-butoxy-3-ethoxyphenyl)methylidene]hydrazinyl]-3-methyl-1-oxobutan-2-yl]-3,4-dichlorobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[1-[2-[(4-butoxy-3-ethoxyphenyl)methylidene]hydrazinyl]-3-methyl-1-oxobutan-2-yl]-3,4-dichlorobenzamide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.22g/cm³
XLogP3:6.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:12
Exact Mass:507.1691619
Heavy Atom Count:34
Complexity:664

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCOC1=C(C=C(C=C1)C=NNC(=O)C(C(C)C)NC(=O)C2=CC(=C(C=C2)Cl)Cl)OCC

Technology Process of N-[1-[2-[(4-butoxy-3-ethoxyphenyl)methylidene]hydrazinyl]-3-methyl-1-oxobutan-2-yl]-3,4-dichlorobenzamide

There total 18 articles about N-[1-[2-[(4-butoxy-3-ethoxyphenyl)methylidene]hydrazinyl]-3-methyl-1-oxobutan-2-yl]-3,4-dichlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3,4′-dihydroxy-5,7-dimethoxyflavone-3-O-β-D-galactopyranosyl-(1→4)-O-β-D-arabinopyranosyl-4′-O-α-L-rhamnopyranoside

: 74-88-4
methyl iodide

: 13403-20-8
O²,O³-dimethyl-D-arabinose

: 7439-05-6
2,3,4-tri-O-methyl-L-rhamnose

: 3615-47-2,5856-22-4,15075-09-9,4060-05-3
2,3,4,6-tetra-O-methyl-D-galactose

: 77316-40-6
5,7-dimethoxy-3-hydroxy-2-(4-hydroxyphenyl)-4H-chromen-4-one

Guidance literature:: 3,4′-dihydroxy-5,7-dimethoxyflavone-3-O-β-D-galactopyranosyl-(1→4)-O-β-D-arabinopyranosyl-4′-O-α-L-rhamnopyranoside; methyl iodide; With silver(l) oxide; In N,N-dimethyl-formamide; for 48h; Reflux;

With sulfuric acid; water; In N,N-dimethyl-formamide;
DOI:10.14233/ajchem.2019.22026

Reference yield:

low-molecular-mass polysaccharide from Cucurbia moschata: low-molecular-mass polysaccharide from Cucurbia moschata

: 6778-35-4
2,3-di-O-methyl-L-arabinose

: 6798-48-7
(2R,3S,4S)-4-Hydroxy-2,3,5-trimethoxy-pentanal

: 5856-20-2
2,4,6-tri-O-methyl-D-galactose

: 3615-47-2,5856-22-4,15075-09-9,4060-05-3
2,3,4,6-tetra-O-methyl-D-galactose

: 18546-13-9
3-O-methyl-L-rhamnose

: C₉H₁₆⁽²⁾H₂O₆

: C₁₀H₁₈O₇

Guidance literature:: low-molecular-mass polysaccharide from Cucurbia moschata; With sodium borodeuteride; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate;

With sodium hydroxide; methyl iodide; In dimethyl sulfoxide; Further stages;
DOI:10.1016/j.carbpol.2020.117090

Reference yield:

Agaricus bisporus fucogalactan RFP-Ab: Agaricus bisporus fucogalactan RFP-Ab

: 74-88-4
methyl iodide

: 7439-05-6,10504-43-5,20735-88-0,22252-42-2,78513-65-2
O²,O³,O⁴-Trimethyl-6-desoxy-L-galactose

: 5856-23-5,27299-06-5,37111-57-2,50721-19-2
O³,O⁴-dimethyl-D-galactose

: 4060-09-7,4060-13-3,4239-83-2,5856-24-6,7330-01-0,40896-77-3,58894-01-2
2.3.4-Tri-O-methyl-D-galactose

: 3615-47-2,5856-22-4,15075-09-9,4060-05-3
2,3,4,6-tetra-O-methyl-D-galactose

Guidance literature:: Agaricus bisporus fucogalactan RFP-Ab; methyl iodide; With sodium hydroxide; In dimethyl sulfoxide;

With formic acid; In water; at 100 ℃; for 6h;
DOI:10.1016/j.carbpol.2011.09.071