2-Methyl-4-phenylsemicarbazide

Base Information

Chemical Name:2-Methyl-4-phenylsemicarbazide
CAS No.:19102-24-0
Molecular Formula:C8H11N3O
Molecular Weight:165.195
Hs Code.:
NSC Number:129977
DSSTox Substance ID:DTXSID10940701
Nikkaji Number:J472.868H
Wikidata:Q82917401
Mol file:19102-24-0.mol

Synonyms:1-Methyl-N-phenylhydrazine-1-carboxamide;19102-24-0;NSC129977;SCHEMBL251878;DTXSID10940701;HMS1782L01;AKOS022637030;NSC-129977;CS-0286837;1-Methyl-N-phenylhydrazine-1-carboximidic acid;Z56855649

Suppliers and Price of 2-Methyl-4-phenylsemicarbazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Methyl-4-phenylsemicarbazide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.237g/cm³
XLogP3:0.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:165.090211983
Heavy Atom Count:12
Complexity:154

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C(=O)NC1=CC=CC=C1)N

Technology Process of 2-Methyl-4-phenylsemicarbazide

There total 6 articles about 2-Methyl-4-phenylsemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 86298-24-0
N-phenyl-1H-benzo[d][1,2,3]triazole-1-carboxamide

: 60-34-4
methylhydrazine

: 19102-24-0
2-methyl-4-phenyl semicarbazide

Guidance literature:: In toluene; at 20 ℃; for 10h; chemoselective reaction;
DOI:10.2298/JSC150126069M

Reference yield:

: 103-71-9
phenyl isocyanate

: 60-34-4
methylhydrazine

: 19102-24-0
2-methyl-4-phenyl semicarbazide

Guidance literature:: With diethyl ether;

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 19102-24-0
2-methyl-4-phenyl semicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; diphenyl phosphoryl azide / toluene / 6 h / Reflux

2: toluene / 10 h / 20 °C

With diphenyl phosphoryl azide; triethylamine; In toluene;
DOI:10.2298/JSC150126069M