1,3-dioxo-1,3-diphenylpropan-2-yl acetate

Base Information

• Chemical Name: 1,3-dioxo-1,3-diphenylpropan-2-yl acetate
• CAS No.: 13054-83-6
• Molecular Formula: C17H14 O4
• Molecular Weight: 282.296

Synonyms:1,3-Propanedione,2-hydroxy-1,3-diphenyl-, acetate (6CI,7CI,8CI);2-Acetoxy-1,3-diphenyl-1,3-propanedione; 2-Hydroxy-1,3-diphenyl-1,3-propanedione,acetate; NSC 156162

Chemical Property of 1,3-dioxo-1,3-diphenylpropan-2-yl acetate

Chemical Property:

• Vapor Pressure: 3.81E-08mmHg at 25°C
• Boiling Point: 445.9°C at 760 mmHg
• Flash Point: 198.4°C
• Density: 1.207g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-dioxo-1,3-diphenylpropan-2-yl acetate

There total 7 articles about 1,3-dioxo-1,3-diphenylpropan-2-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

[bis(acetoxy)iodo]benzene (3240-34-4) + 1,3-diphenylpropanedione (120-46-7,61346-73-4) → 2-acetoxy-1,3-diphenyl-propane-1,3-dione (13054-83-6)

Guidance literature:

With acetic acid; scandium tris(trifluoromethanesulfonate); at 20 ℃; for 6h;

DOI:10.1002/ejoc.201800292

Reference yield: 68.5%

1,3-diphenylpropanedione (120-46-7,61346-73-4) → 2-acetoxy-1,3-diphenyl-propane-1,3-dione (13054-83-6) + benzoic acid (65-85-0,8013-63-6)

Guidance literature:

With [bis(acetoxy)iodo]benzene; In water; acetic acid; at 80 - 100 ℃; for 6h; molar ratio 1:3;

DOI:10.1021/jo00188a031

Reference yield:

α,β-diacetoxy-chalcone (855754-86-8) → 2-acetoxy-1,3-diphenyl-propane-1,3-dione (13054-83-6)

Guidance literature:

With potassium acetate; acetic acid;

DOI:10.1021/ja01861a050

upstream raw materials:

α,β-diacetoxy-chalcone

acetic acid

2-bromo-1,3-diphenylpropane-1,3-dione

acetyl chloride

Downstream raw materials:

α,β-diacetoxy-chalcone

3,5-diphenyl-isoxazol-4-ol

2-hydroxy-1,3-diphenyl-propane-1,3-dione

2,2-Diacetoxy-1,3-diphenylpropan-1,3-dion

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