Hexaphenyldiplumbathiane

Base Information

Chemical Name:Hexaphenyldiplumbathiane
CAS No.:1802-88-6
Molecular Formula:C₃₆H₃₀Pb₂S
Molecular Weight:909.1
Hs Code.:
DSSTox Substance ID:DTXSID40586616
NSC Number:68065
Wikidata:Q82478757

Synonyms:Hexaphenyldiplumbathiane;1802-88-6;DTXSID40586616;NSC68065;NSC-68065

Suppliers and Price of Hexaphenyldiplumbathiane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Hexaphenyldiplumbathiane

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:8
Exact Mass:910.16013
Heavy Atom Count:39
Complexity:551

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Pb](C2=CC=CC=C2)(C3=CC=CC=C3)S[Pb](C4=CC=CC=C4)(C5=CC=CC=C5)C6=CC=CC=C6

Technology Process of Hexaphenyldiplumbathiane

There total 8 articles about Hexaphenyldiplumbathiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1313-82-2
sodium sulfide

: 1153-06-6
triphenyllead(IV) chloride

: 507-09-5
tiolacetic acid

: 1802-88-6
1,1,1,3,3,3-hexaphenyldiplumbathiane

Guidance literature:: With triethylamine; In tetrahydrofuran; THF soln. of triethylamine and thioacetic acid added to a THF soln. of PPh3PbCl and stirred for 4 h; vac. evapn.; extracted with benzene and filtered; added to a suspn. of Na2S; stirred for 3 h; filtered; evapd.; recrystd. from benzene soln. by slow evapn.; elem. anal.;
DOI:10.1016/j.poly.2008.11.033

Reference yield: 67.0%

: 83244-27-3
(C₆H₅)3PbSH

: 7783-06-4
hydrogen sulfide

: 1802-88-6
1,1,1,3,3,3-hexaphenyldiplumbathiane

Guidance literature:: With triethylamine; In tetrahydrofuran; H2S passing (0.5 h); evapn., recrystn. (light petroleum); elem. anal.;
DOI:10.1007/BF02496221

Reference yield: 61.0%

: 1313-82-2
sodium sulfide

: 2117-69-3
diphenyllead(IV) dichloride

: 1802-88-6
1,1,1,3,3,3-hexaphenyldiplumbathiane

Guidance literature:: In tetrahydrofuran; byproducts: NaCl, PbS; addn. of Pb compd. in portions to Na2S suspension under N2, room temp., 30 min; pptn.; stirring, room temp., 14h; pouring into water; filtration; extn. of ppt. with ether; evapn.; drying (vac., 30 min); recrystn. (benzene, hexane); elem. anal.;