2-CHLORO-N-(2,2,6,6-TETRAMETHYLPIPERIDIN-4-YL)ACETAMIDE HYDROCHLORIDE

Base Information

• Chemical Name: 2-CHLORO-N-(2,2,6,6-TETRAMETHYLPIPERIDIN-4-YL)ACETAMIDE HYDROCHLORIDE
• CAS No.: 70804-01-2
• Molecular Formula: C11H22ClN2O+
• Molecular Weight: 232.75
• Mol file: 70804-01-2.mol

Synonyms:

Chemical Property of 2-CHLORO-N-(2,2,6,6-TETRAMETHYLPIPERIDIN-4-YL)ACETAMIDE HYDROCHLORIDE

Chemical Property:

• Vapor Pressure: 3.78E-05mmHg at 25°C
• Boiling Point: 352.7°C at 760 mmHg
• PKA: 13.79±0.60(Predicted)
• Flash Point: 167.1°C
• Density: 1.07g/cm³

Purity/Quality:

99% ^*data from raw suppliers

2-CHLORO-N-(2,2,6,6-TETRAMETHYLPIPERIDIN-4-YL)ACETAMIDE HYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CHLORO-N-(2,2,6,6-TETRAMETHYLPIPERIDIN-4-YL)ACETAMIDE HYDROCHLORIDE

There total 2 articles about 2-CHLORO-N-(2,2,6,6-TETRAMETHYLPIPERIDIN-4-YL)ACETAMIDE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-AMINO-2,2,6,6-TETRAMETHYLPIPERIDINE (36768-62-4) + chloroacetyl chloride (79-04-9) → 2-chloro-N-(2,2,6,6-tetramethylpiperidin-4-yl)acetamide (70804-01-2)

Guidance literature:

In dichloromethane; at 60 ℃; for 8h; Inert atmosphere; Schlenk technique;

DOI:10.1002/cssc.201403204

Reference yield:

→ 2-chloro-N-(2,2,6,6-tetramethylpiperidin-4-yl)acetamide (70804-01-2)

Guidance literature:

entspr. Amin, Cl-CH2-COCl;

DOI:10.1021/jm00195a008

Reference yield:

2-chloro-N-(2,2,6,6-tetramethylpiperidin-4-yl)acetamide (70804-01-2) → 4-[(2-chloroacetyl)amino]-2,2,6,6-tetramethylpiperdine-1-oxyl (36775-23-2)

Guidance literature:

With phosphotungstic acid; dihydrogen peroxide; In water; for 48h; Ambient temperature;

DOI:10.1002/hlca.19800630609

upstream raw materials:

4-AMINO-2,2,6,6-TETRAMETHYLPIPERIDINE

chloroacetyl chloride

Downstream raw materials:

4-[(2-chloroacetyl)amino]-2,2,6,6-tetramethylpiperdine-1-oxyl

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