2,4-Dimethyl-7-(2-methylene-1-oxododecyl)-2H-1,4-benzoxazin-3(4H)-one

Base Information

Chemical Name:2,4-Dimethyl-7-(2-methylene-1-oxododecyl)-2H-1,4-benzoxazin-3(4H)-one
CAS No.:135420-34-7
Molecular Formula:C23H33NO3
Molecular Weight:371.513
Hs Code.:
DSSTox Substance ID:DTXSID80928995
Nikkaji Number:J372.160D
Mol file:135420-34-7.mol

Synonyms:BRN 4331779;2,4-Dimethyl-7-(2-methylene-1-oxododecyl)-2H-1,4-benzoxazin-3(4H)-one;2H-1,4-Benzoxazin-3(4H)-one, 2,4-dimethyl-7-(2-methylene-1-oxododecyl)-;135420-34-7;DTXSID80928995;C23-H33-N-O3;LS-41971;2,4-Dimethyl-7-(2-decylacryloyl)-4H-1,4-benzoxazin-3(2H)-one;2,4-Dimethyl-7-(2-methylidenedodecanoyl)-2H-1,4-benzoxazin-3(4H)-one

Suppliers and Price of 2,4-Dimethyl-7-(2-methylene-1-oxododecyl)-2H-1,4-benzoxazin-3(4H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-Dimethyl-7-(2-methylene-1-oxododecyl)-2H-1,4-benzoxazin-3(4H)-one

Chemical Property:

Vapor Pressure:1.62E-12mmHg at 25°C
Boiling Point:558.8°Cat760mmHg
Flash Point:291.7°C
Density:1.023g/cm³
XLogP3:6.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:11
Exact Mass:371.24604391
Heavy Atom Count:27
Complexity:516

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCC(=C)C(=O)C1=CC2=C(C=C1)N(C(=O)C(O2)C)C

Technology Process of 2,4-Dimethyl-7-(2-methylene-1-oxododecyl)-2H-1,4-benzoxazin-3(4H)-one

There total 5 articles about 2,4-Dimethyl-7-(2-methylene-1-oxododecyl)-2H-1,4-benzoxazin-3(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 51-80-9
bis-(dimethylamino)methane

: 135420-27-8
7-Dodecanoyl-2,4-dimethyl-4H-benzo[1,4]oxazin-3-one

: 135420-34-7
2,4-Dimethyl-7-(2-methylene-dodecanoyl)-4H-benzo[1,4]oxazin-3-one

Guidance literature:: With acetic anhydride; at 90 - 100 ℃; for 3h;

Reference yield:

: 143-07-7
lauric acid

: 135420-34-7
2,4-Dimethyl-7-(2-methylene-dodecanoyl)-4H-benzo[1,4]oxazin-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / polyphosphoric acid / 1.5 h / 110 °C

2: 95 percent / aq. sodium hydroxide / Heating

3: 87 percent / sodium hydrogencarbonate / butan-2-one; H₂O / 8 h / 90 °C

4: 77 percent / acetic anhydride / 3 h / 90 - 100 °C

With sodium hydroxide; PPA; acetic anhydride; sodium hydrogencarbonate; In water; butanone;

Reference yield:

: 21892-80-8
3-methylbenzo[d]oxazol-2(3H)-one

: 135420-34-7
2,4-Dimethyl-7-(2-methylene-dodecanoyl)-4H-benzo[1,4]oxazin-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / polyphosphoric acid / 1.5 h / 110 °C

2: 95 percent / aq. sodium hydroxide / Heating

3: 87 percent / sodium hydrogencarbonate / butan-2-one; H₂O / 8 h / 90 °C

4: 77 percent / acetic anhydride / 3 h / 90 - 100 °C

With sodium hydroxide; PPA; acetic anhydride; sodium hydrogencarbonate; In water; butanone;