N-(2-chloroethyl)cyclohexanamine hydrochloride

Base Information

Chemical Name:N-(2-chloroethyl)cyclohexanamine hydrochloride
CAS No.:50597-62-1
Molecular Formula:C8H16ClN
Molecular Weight:161.6723
Hs Code.:
European Community (EC) Number:864-820-8
NSC Number:29872

Synonyms:N-(2-chloroethyl)cyclohexanamine hydrochloride;50597-62-1;N-(2-chloroethyl)cyclohexanamine;hydrochloride;N-(2-chloroethyl)cyclohexylamine hydrochloride;SCHEMBL10710637;HDGFPODNOGMHTB-UHFFFAOYSA-N;NSC29872;NSC-29872;AKOS026745211;N-(2-chloroethyl)cyclohexanaminehydrochloride;N-2-chloroethyl-cyclohexylamine hydrochloride;EN300-77822;G42318

Suppliers and Price of N-(2-chloroethyl)cyclohexanamine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of N-(2-chloroethyl)cyclohexanamine hydrochloride

Chemical Property:

Vapor Pressure:0.0721mmHg at 25°C
Boiling Point:228.8°Cat760mmHg
Flash Point:92.2°C
Density:0.99g/cm³
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:197.0738049
Heavy Atom Count:11
Complexity:79.3

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC(CC1)NCCCl.Cl

Technology Process of N-(2-chloroethyl)cyclohexanamine hydrochloride

There total 3 articles about N-(2-chloroethyl)cyclohexanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 23605-23-4
2-Chloro-N-cyclohexylacetamide

: 50597-62-1
N-(2-chloroethyl)cyclohexylamine hydrochloride

Guidance literature:: 2-Chloro-N-cyclohexylacetamide; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; for 12h; Inert atmosphere;

With hydrogenchloride; In diethyl ether; for 1h; Inert atmosphere; Reflux;
DOI:10.1002/adsc.201701080

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 50597-62-1
N-(2-chloroethyl)cyclohexylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / dichloromethane / 0 °C / Inert atmosphere

2.1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere; Reflux

With dimethylsulfide borane complex; potassium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/adsc.201701080