3-Phenyl-2H-thiete 1,1-dioxide

Base Information

Chemical Name:3-Phenyl-2H-thiete 1,1-dioxide
CAS No.:25903-17-7
Molecular Formula:C9H8 O2 S
Molecular Weight:180.227
Hs Code.:2902909090
Mol file:25903-17-7.mol

Synonyms:NSC 242973

Suppliers and Price of 3-Phenyl-2H-thiete 1,1-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-PHENYL-2H-THIETE-1,1-DIOXIDE 95.00%
5MG
$ 457.72

Total 8 raw suppliers

Chemical Property of 3-Phenyl-2H-thiete 1,1-dioxide

Chemical Property:

Vapor Pressure:4.99E-06mmHg at 25°C
Boiling Point:393°Cat760mmHg
Flash Point:258.3°C
PSA：42.52000
Density:1.354g/cm³
LogP:2.53670

Purity/Quality:

99% ^*data from raw suppliers

3-PHENYL-2H-THIETE-1,1-DIOXIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Phenyl-2H-thiete 1,1-dioxide

There total 5 articles about 3-Phenyl-2H-thiete 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 77543-73-8
3-phenylthiete 1,1-dioxidebis(triphenylphosphine)platinum⁽⁰⁾

: 670-54-2
ethenetetracarbonitrile

: 25903-17-7
3-phenyl-2H-thiete 1,1-dioxide

: 15711-22-5
Pt(PPh3)2(η2-C(CN)2C(CN)2)

Guidance literature:: In chloroform; soln. of C2(CN)4 in CHCl3 slowly added to soln. of Pt complex in CHCl3, allowed to react for 20 min; filtered, concd., treated with light petroleum;
DOI:10.1016/S0022-328X(00)82443-2

Reference yield:

: 66982-50-1
3-phenyl-3-hydroxythietane 1,1-dioxide

: 25903-17-7
3-phenyl-2H-thiete 1,1-dioxide

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01961

Reference yield:

: 100-59-4
phenylmagnesium chloride

: 25903-17-7
3-phenyl-2H-thiete 1,1-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 1 h / -30 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

3: triethylamine; methanesulfonyl chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With methanesulfonyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.8b01961