2-CYCLOHEXYLAMINOMETHYL-PHENOL

Base Information

• Chemical Name: 2-CYCLOHEXYLAMINOMETHYL-PHENOL
• CAS No.: 62984-53-6
• Molecular Formula: C13H20NO+
• Molecular Weight: 205.3
• Hs Code.: 2922299090
• Mol file: 62984-53-6.mol

Synonyms:HMS1583K11;2-((cyclohexylamino)methyl)phenol;

Chemical Property of 2-CYCLOHEXYLAMINOMETHYL-PHENOL

Chemical Property:

• Vapor Pressure: 5.33E-05mmHg at 25°C
• Boiling Point: 337.5°Cat760mmHg
• Flash Point: 117.4°C
• PSA: 32.26000
• Density: 1.07g/cm³
• LogP: 3.20540

Purity/Quality:

99%min ^*data from raw suppliers

2-[(cyclohexylamino)methyl]phenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CYCLOHEXYLAMINOMETHYL-PHENOL

There total 4 articles about 2-CYCLOHEXYLAMINOMETHYL-PHENOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

cyclohexylamine (108-91-8,157973-60-9) + salicylaldehyde (90-02-8) → 2-((cyclohexylamino)methyl)phenol (62984-53-6)

Guidance literature:

cyclohexylamine; salicylaldehyde; In methanol; at 20 ℃; for 3h; Inert atmosphere;

With magnetic borohydride exchange resin; In methanol; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1002/chem.201300358

Reference yield: 99.0%

C13H17NO*H(1+) → 2-((cyclohexylamino)methyl)phenol (62984-53-6)

Guidance literature:

With [Cp*Ir-(4,4’-dimethoxyl-2,2’-bipyridine)(OH₂)][SO₄]; 1-Benzyl-1,4-dihydronicotinamide; In aq. phosphate buffer; at 20 ℃; for 24h; pH=7;

DOI:10.1002/cctc.201601307

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + cyclohexylamine (108-91-8,157973-60-9) + phenol (108-95-2,27073-41-2) → 2-((cyclohexylamino)methyl)phenol (62984-53-6)

Guidance literature:

DOI:10.1021/ja01126a050

upstream raw materials:

formaldehyd

cyclohexylamine

phenol

salicylaldehyde

Downstream raw materials:

salicylic alcohol

Refernces

• 1、 Choi, Dubok,Yu, Sunjong,Baek, Seung Ho,Kang, Yoon-Ho,Chang, Young-Cheol,Cho, Hoon. "Synthesis and algicidal activity of new dichlorobenzylamine derivatives against harmful red tides". . p. 463 - 476. Retrieved 2016/07/30.