5-Chloro-2-phenyl-1,3-indandione

Base Information

Chemical Name:5-Chloro-2-phenyl-1,3-indandione
CAS No.:1470-36-6
Molecular Formula:C15H9 Cl O2
Molecular Weight:256.6838
Hs Code.:
DSSTox Substance ID:DTXSID00933001

Synonyms:1470-36-6;BRN 2112627;5-Chloro-2-phenyl-1,3-indandione;1,3-Indandione, 5-chloro-2-phenyl-;SCHEMBL14939892;DTXSID00933001;5-Chloro-2-phenyl-1H-indene-1,3(2H)-dione

Suppliers and Price of 5-Chloro-2-phenyl-1,3-indandione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 5-Chloro-2-phenyl-1,3-indandione

Chemical Property:

Vapor Pressure:2.71E-08mmHg at 25°C
Boiling Point:450.1°Cat760mmHg
Flash Point:189.6°C
Density:1.367g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:256.0291072
Heavy Atom Count:18
Complexity:360

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2C(=O)C3=C(C2=O)C=C(C=C3)Cl

Technology Process of 5-Chloro-2-phenyl-1,3-indandione

There total 3 articles about 5-Chloro-2-phenyl-1,3-indandione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-82-2
phenylacetic acid

: 118-45-6
4-chlorophthalic anhydride

: 1470-36-6
5-chloro-2-phenylindan-1,3-dione

Guidance literature:: With sodium acetate; at 220 - 240 ℃; Erwaermen des Reaktionsprodukts mit methanol. Natriummethylat;

Reference yield:

: 89-20-3
4-chlorophthalic acid

: 1470-36-6
5-chloro-2-phenylindan-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: 90 percent / acetic anhydride / 1 h / Heating

2.1: Ac₂O; Et₃N / 1.5 h / Heating

2.2: NaOMe / methanol / 0.75 h

With acetic anhydride; triethylamine;
DOI:10.1016/j.bmcl.2005.11.041