4-(1-Methylvinyl)cyclohex-1-ene-1-methyl formate

Base Information

• Chemical Name: 4-(1-Methylvinyl)cyclohex-1-ene-1-methyl formate
• CAS No.: 29621-55-4
• Molecular Formula: C₁₁H₁₆O₂
• Molecular Weight: 180.247
• European Community (EC) Number: 249-731-9
• DSSTox Substance ID: DTXSID20952092
• Nikkaji Number: J286.912H
• Mol file: 29621-55-4.mol

Synonyms:29621-55-4;4-(1-Methylvinyl)cyclohex-1-ene-1-methyl formate;EINECS 249-731-9;SCHEMBL21302589;DTXSID20952092;4-(1-Methylethenyl)-1-cyclohexene-1-methanol formate;[4-(prop-1-en-2-yl)cyclohex-1-en-1-yl]methyl formate

Chemical Property of 4-(1-Methylvinyl)cyclohex-1-ene-1-methyl formate

Chemical Property:

• Vapor Pressure: 0.0381mmHg at 25°C
• Refractive Index: 1.474
• Boiling Point: 240.4°Cat760mmHg
• Flash Point: 101.1°C
• Density: 0.976g/cm³
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 180.115029749
• Heavy Atom Count: 13
• Complexity: 228

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=C)C1CCC(=CC1)COC=O

Technology Process of 4-(1-Methylvinyl)cyclohex-1-ene-1-methyl formate

There total 5 articles about 4-(1-Methylvinyl)cyclohex-1-ene-1-methyl formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(-)-perillyl alcohol + formyl acetic anhydride (2258-42-6) → (-)-perillyl formate (29621-55-4)

Guidance literature:

With pyridine; In dichloromethane; for 0.833333h;

DOI:10.1080/00397919508011375

Reference yield: 88.0%

(-)-perillyl alcohol (536-59-4,18457-55-1) + (formyloxy)(acetoxy)phenylmethane (113388-44-6) → perillyl formate (72506-01-5,29621-55-4)

Guidance literature:

With sodium hydrogencarbonate; In neat (no solvent); at 60 ℃; for 16h;

DOI:10.1016/j.tet.2018.09.014

Reference yield:

formic acid (64-18-6) + (-)-β-Pinenoxid (875-08-1,6931-54-0,18680-30-3,23516-38-3,32162-29-1,56246-58-3) → perillyl formate (72506-01-5,29621-55-4) + (S)-(4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl acetate (15111-96-3,56452-54-1,35907-08-5)

Guidance literature:

With acetic anhydride; Yield given. Multistep reaction. Yields of byproduct given; 1) 18 h, r.t., 2) 18 h, reflux;

upstream raw materials:

formic acid

(-)-β-Pinenoxid

acetic anhydride

β-pinene oxide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 29621-55-4 4-(1-methylvinyl)cyclohex-1-ene-1-methyl formate

Send

Send

Metric Ton KG G Pound L ML

Send

Send