Methyldecyl sulfone

Base Information

• Chemical Name: Methyldecyl sulfone
• CAS No.: 54863-62-6
• Molecular Formula: C11H24O2S
• Molecular Weight: 220.376
• Hs Code.: 2904100000
• Mol file: 54863-62-6.mol

Synonyms:decyl methyl sulfone;1-methanesulfonyl-decane;Decylmethylsulfon;

Chemical Property of Methyldecyl sulfone

Chemical Property:

• Vapor Pressure: 0.000292mmHg at 25°C
• Boiling Point: 331.9°C at 760 mmHg
• Flash Point: 163.3°C
• PSA: 42.52000
• Density: 0.953g/cm³
• LogP: 4.25250

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methyldecyl sulfone

There total 10 articles about Methyldecyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-(methylthio)decane (22438-39-7) → 1-(methylsulfonyl)decane (54863-62-6)

Guidance literature:

With oxygen; layered double hydroxide-OsO₄; In phosphate buffer; tert-butyl alcohol; at 55 ℃; for 12h; under 750.06 Torr; pH=10.4;

DOI:10.1039/b212749k

Reference yield: 88.0%

1-(methylthio)decane (22438-39-7) → decyl methyl sulfoxide (3079-28-5) + 1-(methylsulfonyl)decane (54863-62-6)

Guidance literature:

With oxygen; cis-{RuCl₂(Me₂SO)4}; In isopropyl alcohol; at 100 ℃; for 16h; under 5171.5 Torr; Kinetics; Thermodynamic data; Product distribution; E_a, ΔS⁺; further dihaloruthenium(II) complex catalysts; further sulfide substrates; further solvent; variation of temperature;

DOI:10.1021/ja00323a020

Reference yield: 19.0%

dimethylsulfite (616-42-2) + Iododecane (2050-77-3) → 1-(methylsulfonyl)decane (54863-62-6)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; 1,1,3,3-Tetramethyldisiloxane; tetrabutylammomium bromide; In 1,4-dioxane; at 120 ℃; for 18h; Inert atmosphere;

upstream raw materials:

methyl iodide

1-(methylthio)decane

2-n-hexyl sulfolane

4-(Decane-1-sulfonyl)-pyridine