N,N-dimethyl-P,P-diphenylphosphinothioic amide

Base Information

Chemical Name:N,N-dimethyl-P,P-diphenylphosphinothioic amide
CAS No.:17513-68-7
Molecular Formula:C14H16NPS
Molecular Weight:261.327
Hs Code.:
DSSTox Substance ID:DTXSID50938627
Nikkaji Number:J480.253E
Wikidata:Q82914993

Synonyms:N,N-dimethyl-P,P-diphenylphosphinothioic amide;17513-68-7;AI3-61525;Phosphinothioic amide, N,N-dimethyl-P,P-diphenyl-;Thiophosphinic acid, diphenyl-, dimethylamide;DTXSID50938627;LWSCOQLJATUVES-UHFFFAOYSA-N;STK106071;AKOS005397693

Suppliers and Price of N,N-dimethyl-P,P-diphenylphosphinothioic amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N,N-DIMETHYL-P,P-DIPHENYLPHOSPHINOTHIOIC AMIDE 95.00%
5MG
$ 503.13

Total 0 raw suppliers

Chemical Property of N,N-dimethyl-P,P-diphenylphosphinothioic amide

Chemical Property:

PSA：45.14000
LogP:3.24410
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:261.07410769
Heavy Atom Count:17
Complexity:256

Purity/Quality:: N,N-DIMETHYL-P,P-DIPHENYLPHOSPHINOTHIOIC AMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)P(=S)(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of N,N-dimethyl-P,P-diphenylphosphinothioic amide

There total 2 articles about N,N-dimethyl-P,P-diphenylphosphinothioic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1253395-46-8
3-(diphenylphosphino)-1-methyl-2-phenyl-1H-imidazol-3-ium bromide

: 124-40-3
dimethyl amine

: 3475-07-8
N-methyl-2-phenyl-1H-imidazole

: 17513-68-7
diphenyl-thiophosphinic acid dimethylamide

Guidance literature:: 3-(diphenylphosphino)-1-methyl-2-phenyl-1H-imidazol-3-ium bromide; dimethyl amine; In diethyl ether; at -30 - 16 ℃; Inert atmosphere;

With sulfur; In diethyl ether; for 0.25h; Heating; Inert atmosphere;
DOI:10.1021/jo101177h

Reference yield:

: 17513-68-7
diphenyl-thiophosphinic acid dimethylamide

Guidance literature:: /BRN= 2804569/;

Reference yield: 78.0%

: 17513-68-7
diphenyl-thiophosphinic acid dimethylamide

: 74-88-4
methyl iodide

: 90602-04-3
C₁₅H₁₈NPS

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; In various solvent(s); at -10 ℃;
DOI:10.1016/S0040-4039(00)99936-2