2,2,4,4,6,6-hexamethoxy-1,3,5,2,4,6-trioxatrisilinane

Base Information

• Chemical Name: 2,2,4,4,6,6-hexamethoxy-1,3,5,2,4,6-trioxatrisilinane
• CAS No.: 110920-52-0
• Molecular Formula: C6H18 O9 Si3
• Molecular Weight: 318.46
• Mol file: 110920-52-0.mol

Synonyms:Cyclotrisiloxane,hexamethoxy- (9CI); Silicic acid (H6Si3O9), hexamethyl ester

Chemical Property of 2,2,4,4,6,6-hexamethoxy-1,3,5,2,4,6-trioxatrisilinane

Chemical Property:

• Vapor Pressure: 2.23mmHg at 25°C
• Boiling Point: 167.5°Cat760mmHg
• Flash Point: 49.1°C
• Density: 1.16g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2,4,4,6,6-hexamethoxy-1,3,5,2,4,6-trioxatrisilinane

There total 3 articles about 2,2,4,4,6,6-hexamethoxy-1,3,5,2,4,6-trioxatrisilinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3-dimethoxy-6-oxa-3-silabicyclo[3.1.0]hexane (88794-58-5) → methanol (67-56-1) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + Dimethyl ether (115-10-6,157621-61-9) + 2,2,4,4-Tetramethoxy-[1,3,2,4]dioxadisiletane (129575-55-9) + 2,2,4,4,6,6-hexamethoxycyclotrisiloxane (110920-52-0) + buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2)

Guidance literature:

at 700 ℃; under 0.1 Torr; Product distribution; trapping of the products in argon cryogenic matrices at 12 K; various temperature and pressure;

DOI:10.1016/S0022-328X(98)00726-8

Reference yield:

trimethyl orthoformate (149-73-5) → 2,2,4,4,6,6-hexamethoxycyclotrisiloxane (110920-52-0)

Guidance literature:

With hexachlorocyclosiloxane; In pentane; for 72h; Ambient temperature;

Reference yield:

3,3-dimethoxy-6-oxa-3-silabicyclo[3.1.0]hexane (88794-58-5) → 2,2,4,4-Tetramethoxy-[1,3,2,4]dioxadisiletane (129575-55-9) + 2,2,4,4,6,6-hexamethoxycyclotrisiloxane (110920-52-0)

Guidance literature:

at 25 - 1100 ℃; Product distribution;

DOI:10.1016/0022-328X(90)80019-V

upstream raw materials:

3,3-dimethoxy-6-oxa-3-silabicyclo[3.1.0]hexane

trimethyl orthoformate