n-(2-Bromophenyl)pyridine-3-carboxamide

Base Information

Chemical Name:n-(2-Bromophenyl)pyridine-3-carboxamide
CAS No.:75075-29-5
Molecular Formula:C12H9BrN2O
Molecular Weight:277.12
Hs Code.:
NSC Number:131169
DSSTox Substance ID:DTXSID10299529
Nikkaji Number:J1.250.361J
Wikidata:Q82041987

Synonyms:n-(2-bromophenyl)pyridine-3-carboxamide;75075-29-5;NSC131169;N-(2-Bromophenyl)-3-pyridinecarboxamide;DTXSID10299529;AKOS000176042;NSC-131169;N-(2-bromophenyl)pyri-dine-3-carboxamide;Z27784736

Suppliers and Price of n-(2-Bromophenyl)pyridine-3-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of n-(2-Bromophenyl)pyridine-3-carboxamide

Chemical Property:

Vapor Pressure:0.000649mmHg at 25°C
Boiling Point:309.2°Cat760mmHg
Flash Point:140.8°C
Density:1.559g/cm³
XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:275.98983
Heavy Atom Count:16
Complexity:247

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)NC(=O)C2=CN=CC=C2)Br

Technology Process of n-(2-Bromophenyl)pyridine-3-carboxamide

There total 3 articles about n-(2-Bromophenyl)pyridine-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 10400-19-8
3-pyridinecarbonyl chloride

: 615-36-1
2-bromoaniline

: 75075-29-5
N-(2-bromophenyl)-3-pyridinecarboxamide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1021/jo051927q

Reference yield:

: 59-67-6
nicotinic acid

: 75075-29-5
N-(2-bromophenyl)-3-pyridinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / Heating

2: Py / 0 - 20 °C

With pyridine; thionyl chloride; 1: Substitution / 2: Acylation;
DOI:10.1021/jo9909498