8-Methyl-3-methylene-8-aza-bicyclo[3.2.1]octane

Base Information

Chemical Name:8-Methyl-3-methylene-8-aza-bicyclo[3.2.1]octane
CAS No.:99838-33-2
Molecular Formula:C₉H₁₅N
Molecular Weight:137.225
Hs Code.:2933990090
Mol file:99838-33-2.mol

Synonyms:8-Methyl-3-methylene-8-azabicyclo(3.2.1)octane;3-methylenetropane;

Suppliers and Price of 8-Methyl-3-methylene-8-aza-bicyclo[3.2.1]octane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
8-METHYL-3-METHYLENE-8-AZA-BICYCLO[3.2.1]OCTANE 95.00%
10G
$ 4152.23

American Custom Chemicals Corporation
8-METHYL-3-METHYLENE-8-AZA-BICYCLO[3.2.1]OCTANE 95.00%
5G
$ 2939.48

Total 2 raw suppliers

Chemical Property of 8-Methyl-3-methylene-8-aza-bicyclo[3.2.1]octane

Chemical Property:

Vapor Pressure:0.652mmHg at 25°C
Boiling Point:186.8°Cat760mmHg
Flash Point:59.3°C
PSA：3.24000
Density:0.96g/cm³
LogP:1.73710

Purity/Quality:

98% ^*data from raw suppliers

8-METHYL-3-METHYLENE-8-AZA-BICYCLO[3.2.1]OCTANE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 8-Methyl-3-methylene-8-aza-bicyclo[3.2.1]octane

There total 2 articles about 8-Methyl-3-methylene-8-aza-bicyclo[3.2.1]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532-24-1
tropinone

: 1779-49-3
Methyltriphenylphosphonium bromide

: 99838-33-2
8-methyl-3-methylene-8-azabicyclo<3.2.1>octane

Guidance literature:: With potassium tert-butylate; Yield given. Multistep reaction; 1.) THF, 15 h, 2.) THF, 15 h;
DOI:10.1021/jo00355a004

Reference yield:

: 122601-47-2
3α-hydroxymethyltropane tosylate

: 99838-33-2
8-methyl-3-methylene-8-azabicyclo<3.2.1>octane

: 142892-46-4
3-methyltrop-2-ene

: 142892-48-6
3α-methyltropan-3β-ol

: 142892-47-5
3β,8-dimethyl-8-azabicyclo<3.2.1>oct-3α-ol

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; water; at 105 ℃; for 82.5h; Rate constant; Thermodynamic data; or (i-Pr)2NEt; other reaction temperatures and times, ΔH(excit.), ΔS(excit.);
DOI:10.1016/S0040-4020(01)81578-7