Iron,tricarbonyl[(1,2,3,4-h)-2,3-dimethyl-1,3-butadiene]-

Base Information

Chemical Name:Iron,tricarbonyl[(1,2,3,4-h)-2,3-dimethyl-1,3-butadiene]-
CAS No.:31741-56-7
Molecular Formula:C₉H₁₀FeO₃
Molecular Weight:222.024
Hs Code.:

Synonyms:Iron,tricarbonyl(2,3-dimethyl-1,3-butadiene)- (8CI); 2,3-Dimethylbutadieneirontricarbonyl; Tricarbonyl(2,3-dimethyl-1,3-butadiene)iron;Tricarbonyl(2,3-dimethylbutadiene)iron; Tricarbonyl(h4-2,3-dimethyl-1,3-butadiene)iron

Suppliers and Price of Iron,tricarbonyl[(1,2,3,4-h)-2,3-dimethyl-1,3-butadiene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Iron,tricarbonyl[(1,2,3,4-h)-2,3-dimethyl-1,3-butadiene]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Iron,tricarbonyl[(1,2,3,4-h)-2,3-dimethyl-1,3-butadiene]-

There total 2 articles about Iron,tricarbonyl[(1,2,3,4-h)-2,3-dimethyl-1,3-butadiene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: [2-[(dimethylamino)methyl]phenyl]phenylsilanediyliron⁽⁰⁾ tetracarbonyl

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 31741-56-7,52993-10-9
tricarbonyl(2,3-dimethylbuta-1,3-diene)iron

: 38894-55-2,14881-58-4
1,2-bis(diphenylphosphino)ethaneiron(0) tricarbonyl

Guidance literature:: In toluene; byproducts: C6H5Si(C6H9)C6H4CH2NMe2; Irradiation (UV/VIS); Ar-atmosphere; irradn. (room temp., 5 h); elem. anal.;
DOI:10.1021/om00004a020

Reference yield: 1.0%

: [2-[(dimethylamino)methyl]phenyl]phenylsilanediyliron⁽⁰⁾ tetracarbonyl

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 17685-52-8
triiron dodecarbonyl

: 31741-56-7,52993-10-9
tricarbonyl(2,3-dimethylbuta-1,3-diene)iron

Guidance literature:: In toluene; byproducts: C6H5Si(C6H9)C6H4CH2NMe2; Irradiation (UV/VIS); Ar-atmosphere; irradn. (room temp., 6 h); evapn., chromy. (SiO2, pentane / ether = 90 : 10); elem. anal.;
DOI:10.1021/om00004a020

Reference yield: 85.0%

: 31741-56-7,52993-10-9
tricarbonyl(2,3-dimethylbuta-1,3-diene)iron

: 98-88-4
benzoyl chloride

: {C₄H₃(CH₃)2(COC₆H₅)}Fe(CO)3

Guidance literature:: With aluminium trichloride; In dichloromethane; Ar-atmosphere; addn. of acyl chloride to AlCl3 suspn. (0°C), stirring (10 min.), addn. of Fe-complex, stirring (1 h at 0°C); pouring onto water and ice, extn. of aq. layer (ether), washing of combined org. layer (aq. NaHCO3), drying (MgSO4), evapn. (reduced pressure), chromy. (SiO2, hexane/ether); elem. anal.;