4-Methoxy-trans-beta-chlorostyrene

Base Information

Chemical Name:4-Methoxy-trans-beta-chlorostyrene
CAS No.:18684-94-1
Molecular Formula:C9H9ClO
Molecular Weight:168.623
Hs Code.:
UNII:3NLX1V50KT
DSSTox Substance ID:DTXSID001270064
Nikkaji Number:J1.272.808E,J1.379.379D
Wikidata:Q27257769
Mol file:18684-94-1.mol

Synonyms:4-Methoxy-trans-beta-chlorostyrene;18684-94-1;UNII-3NLX1V50KT;3NLX1V50KT;Anisole, p-(2-chlorovinyl)-, (E)-;(E)-1-(2-Chlorovinyl)-4-methoxybenzene;1-((E)-2-Chlorovinyl)-4-methoxybenzene;1-[(E)-2-chloroethenyl]-4-methoxybenzene;trans-beta-Chloro-4-methoxystyrene;1-(2-Chloroethenyl)-4-methoxybenzene, (1E)-;1-(-2-CHLORO-VINYL)-4-METHOXY-BENZENE;18684-79-2;4-(2-Chlorovinyl)anisole;4-[(E)-2-Chlorovinyl]anisole;SCHEMBL10955396;XURGFZNIMRDEBA-VOTSOKGWSA-N;DTXSID001270064;AKOS006276233;4-(2-CHLOROVINYL)ANISOLE, TRANS-;(1E)-1-(2-chloroethenyl)-4-methoxybenzene;1-[(1E)-2-Chloroethenyl]-4-methoxybenzene;METHOXY-TRANS-BETA-CHLOROSTYRENE, 4-;TRANS-.BETA.-CHLORO-4-METHOXYSTYRENE;TRANS-.BETA.-CHLORO-P-METHOXYSTYRENE;Q27257769;BENZENE, 1-((1E)-2-CHLOROETHENYL)-4-METHOXY-;BENZENE, 1-(2-CHLOROETHENYL)-4-METHOXY-, (E)-

Suppliers and Price of 4-Methoxy-trans-beta-chlorostyrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 4-Methoxy-trans-beta-chlorostyrene

Chemical Property:

Vapor Pressure:0.0137mmHg at 25°C
Boiling Point:267°Cat760mmHg
Flash Point:118.7°C
PSA：9.23000
Density:1.112g/cm³
LogP:2.90470
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:168.0341926
Heavy Atom Count:11
Complexity:126

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C=CCl
Isomeric SMILES:COC1=CC=C(C=C1)/C=C/Cl

Technology Process of 4-Methoxy-trans-beta-chlorostyrene

There total 31 articles about 4-Methoxy-trans-beta-chlorostyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 943-89-5
(E)-3-(4-methoxyphenyl)acrylic acid

: 18684-94-1
1-[(E)-2-chlorovinyl]-4-methoxybenzene

Guidance literature:: With N-chloro-succinimide; triethylamine; In dichloromethane; at 20 ℃; for 0.0833333h;
DOI:10.1021/jo025868h

Reference yield: 88.0%

: 593-71-5
Chloroiodomethane

: 2746-25-0
p-Methoxybenzyl bromide

: 18684-94-1
1-[(E)-2-chlorovinyl]-4-methoxybenzene

Guidance literature:: Chloroiodomethane; With sodium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; at -78 ℃; Inert atmosphere; Darkness;

p-Methoxybenzyl bromide; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; optical yield given as %de; stereoselective reaction; Inert atmosphere;

Reference yield: 80.0%

: 28540-81-0
(E) 2-iodo-1-chloroethylene

: 5720-07-0
4-methoxyphenylboronic acid

: 4705-34-4,15638-14-9,34480-01-8,112246-67-0,2510-75-0
1,2-bis(4-methoxyphenyl)ethene

: 2132-80-1
4,4'-Dimethoxybiphenyl

: 18684-94-1
1-[(E)-2-chlorovinyl]-4-methoxybenzene

Guidance literature:: With potassium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 60 ℃; for 10h;
DOI:10.1016/j.tet.2004.08.006