3-benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane-2,4-dione

Base Information

Chemical Name:3-benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane-2,4-dione
CAS No.:17783-46-9
Molecular Formula:C14H16 N2 O2
Molecular Weight:244.293
Hs Code.:

Synonyms:2,5-Pyrrolidinedicarboximide,N-benzyl-1-methyl- (8CI); 3-Benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane-2,4-dione;NSC 145984

Suppliers and Price of 3-benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane-2,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 7 raw suppliers

Chemical Property of 3-benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane-2,4-dione

Chemical Property:

Vapor Pressure:6.89E-08mmHg at 25°C
Boiling Point:438.5°Cat760mmHg
Flash Point:207.1°C
Density:1.244g/cm³

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane-2,4-dione

There total 4 articles about 3-benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: diethyl cis-1-methylpyrrolidine-2,5-dicarboxylate

: 100-46-9
benzylamine

: 17783-46-9
3-benzyl-2,4-dioxo-8-methyl-3,8-diazabicyclo-(3.2.1)octane

Guidance literature:: diethyl cis-1-methylpyrrolidine-2,5-dicarboxylate; benzylamine; In xylene; for 16h; Heating / reflux;

at 220 ℃; for 18h; Neat (no solvent);

Reference yield: 34.0%

: 52321-02-5
diethyl cis-1-methylpyrrolidine-2,5-dicarboxylate

: 100-46-9
benzylamine

: 17783-46-9
3-benzyl-2,4-dioxo-8-methyl-3,8-diazabicyclo-(3.2.1)octane

Guidance literature:: In xylene; at 220 ℃; Reflux;

Reference yield:

: 869-10-3
diethyl 2,5-dibromoadipate

: 17783-46-9
3-benzyl-2,4-dioxo-8-methyl-3,8-diazabicyclo-(3.2.1)octane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 18 h / 0 - 20 °C

2: xylene / 34 h / 220 °C / Heating / reflux

In tetrahydrofuran; xylene;