3-Benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane

Base Information

Chemical Name:3-Benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane
CAS No.:17783-48-1
Molecular Formula:C14H20N2
Molecular Weight:216.326
Hs Code.:
DSSTox Substance ID:DTXSID301203903

Synonyms:3-benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane;17783-48-1;SCHEMBL1022483;DTXSID301203903;MFCD27923786;SY037204;CS-0448391;3benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane;A924844;3-benzyl-8-methyl-3,8-diazabicyclo-[3.2.1]octane;8-Methyl-3-(phenylmethyl)-3,8-diazabicyclo[3.2.1]octane

Suppliers and Price of 3-Benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:216.162648646
Heavy Atom Count:16
Complexity:221

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2CCC1CN(C2)CC3=CC=CC=C3

Technology Process of 3-Benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane

There total 4 articles about 3-Benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 17783-46-9
3-benzyl-2,4-dioxo-8-methyl-3,8-diazabicyclo-(3.2.1)octane

: 17783-48-1
3-benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane

Guidance literature:: 3-benzyl-2,4-dioxo-8-methyl-3,8-diazabicyclo-(3.2.1)octane; With lithium aluminium tetrahydride; In 1,4-dioxane; for 18h; Heating / reflux;

With water; In 1,4-dioxane; for 0.333333h;

Reference yield:

: 869-10-3
diethyl 2,5-dibromoadipate

: 17783-48-1
3-benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 18 h / 0 - 20 °C

2.1: xylene / 34 h / 220 °C / Heating / reflux

3.1: lithium aluminium tetrahydride / 1,4-dioxane / 18 h / Heating / reflux

3.2: 0.33 h

With lithium aluminium tetrahydride; In tetrahydrofuran; 1,4-dioxane; xylene;

Reference yield:

: diethyl cis-1-methylpyrrolidine-2,5-dicarboxylate

: 100-46-9
benzylamine

: 17783-48-1
3-benzyl-8-methyl-3,8-diazabicyclo[3.2.1]octane

Guidance literature:: Multi-step reaction with 2 steps

1.1: xylene / 34 h / 220 °C / Heating / reflux

2.1: lithium aluminium tetrahydride / 1,4-dioxane / 18 h / Heating / reflux

2.2: 0.33 h

With lithium aluminium tetrahydride; In 1,4-dioxane; xylene;