N-(2-Nitro-4,5-dichlorophenyl)-D-glucamine

Base Information

• Chemical Name: N-(2-Nitro-4,5-dichlorophenyl)-D-glucamine
• CAS No.: 108751-29-7
• Molecular Formula: C₁₂H₁₆Cl₂N₂O₇
• Molecular Weight: 371.174
• DSSTox Substance ID: DTXSID50910867
• Mol file: 108751-29-7.mol

Synonyms:BRN 3221309;N-(2-Nitro-4,5-dichlorophenyl)-D-glucamine;Sorbitol, 1-deoxy-1-(4,5-dichloro-2-nitroanilino)-;D-Glucitol, 1-deoxy-1-(4,5-dichloro-2-nitroanilino)-;4-12-00-01679 (Beilstein Handbook Reference);108751-29-7;C12H16Cl2N2O7;DTXSID50910867;C12-H16-Cl2-N2-O7;LS-145686;1-Deoxy-1-(4,5-dichloro-2-nitroanilino)hexitol

Chemical Property of N-(2-Nitro-4,5-dichlorophenyl)-D-glucamine

Chemical Property:

• Vapor Pressure: 9.67E-22mmHg at 25°C
• Boiling Point: 719.7°Cat760mmHg
• Flash Point: 389.1°C
• Density: 1.716g/cm³
• XLogP3: 0.4
• Hydrogen Bond Donor Count: 6
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 7
• Exact Mass: 370.0334562
• Heavy Atom Count: 23
• Complexity: 387

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=C(C(=CC(=C1Cl)Cl)[N+](=O)[O-])NCC(C(C(C(CO)O)O)O)O

Technology Process of N-(2-Nitro-4,5-dichlorophenyl)-D-glucamine

There total 6 articles about N-(2-Nitro-4,5-dichlorophenyl)-D-glucamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-glucose (50-99-7) → 1-(4,5-dichloro-2-nitro-anilino)-1-deoxy-D-glucitol (108751-29-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Raney nickel; ammonia / 85 °C / 102971 Torr / Hydrogenation

With ammonia; nickel;

DOI:10.1021/ja01168a014

Reference yield:

D-Galactose (59-23-4) → 1-(4,5-dichloro-2-nitro-anilino)-D-1-deoxy-galactitol (108751-29-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Raney nickel; ammonia / 85 °C / 102971 Torr / Hydrogenation

With ammonia; nickel;

DOI:10.1021/ja01168a014

Reference yield:

1-Amino-1-deoxy-D-glucitol (488-43-7) + 1,2-dichloro-4,5-dinitrobenzene (6306-39-4) → 1-(4,5-dichloro-2-nitro-anilino)-1-deoxy-D-glucitol (108751-29-7)

Guidance literature:

DOI:10.1021/ja01168a014

upstream raw materials:

1,2-dichloro-4,5-dinitrobenzene

1-Amino-1-deoxy-D-glucitol

D-glucose

1-amino-1-deoxy-D-galactitol