1,2,3-tris(benzyloxy)-5-nitrobenzene

Base Information

Chemical Name:1,2,3-tris(benzyloxy)-5-nitrobenzene
CAS No.:6274-77-7
Molecular Formula:C₂₇H₂₃NO₅
Molecular Weight:441.483
Hs Code.:

Synonyms:Benzene,1,2,3-tris(benzyloxy)-5-nitro- (6CI); 1,2,3-Tris(benzyloxy)-5-nitrobenzene;3,4,5-Tribenzyloxynitrobenzene; NSC 37464

Suppliers and Price of 1,2,3-tris(benzyloxy)-5-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1,2,3-tris(benzyloxy)-5-nitrobenzene

Chemical Property:

Vapor Pressure:9.68E-15mmHg at 25°C
Boiling Point:622.4°Cat760mmHg
Flash Point:236.3°C
Density:1.242g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2,3-tris(benzyloxy)-5-nitrobenzene

There total 10 articles about 1,2,3-tris(benzyloxy)-5-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 55020-64-9
1,2,3-tris-benzyloxybenzene

: 6625-45-2
2,6-bis-benzyloxy-[1,4]benzoquinone

: 6274-77-7
1,2,3-tris-benzyloxy-5-nitrobenzene

Guidance literature:: With nitric acid; acetic acid; for 15h;
DOI:10.1016/S0040-4020(03)00862-7

Reference yield:

: 87-66-1
2-hydroxyresorcinol

: 6274-77-7
1,2,3-tris-benzyloxy-5-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / K₂CO₃ / acetone / 15 h / Heating

2: 51 percent / HOAc; aq. HNO₃ / 15 h

With nitric acid; potassium carbonate; acetic acid; In acetone;
DOI:10.1016/S0040-4020(03)00862-7

Reference yield:

: 100-39-0
benzyl bromide

: 6274-77-7
1,2,3-tris-benzyloxy-5-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / K₂CO₃ / acetone / 1.) stirring, 30 min, 2.) reflux, 8 h

2: nitric acid / acetic acid / Ambient temperature

With nitric acid; potassium carbonate; In acetic acid; acetone;
DOI:10.1002/ardp.19943270411